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1.
Measurement of the thermal transport properties of dielectric thin films using the micro-Raman method 总被引：1，自引：0，他引：1
The micro-Raman method is a non-contact and non-destructive method for thermal conductivity measurement. To reduce the measurement error induced by the poor fit of the basic equation of the original micro-Raman method, we developed a new basic equation for the heat source ofa Gaussian laser beam. Based on the new basic equation, an analytical heat transfer model has been built to extend the original micro-Raman method to thin films with submicrometer- or nanometer-scale thickness. Experiments were performed to measure the thermal conductivity of dielectric thin films with submicrometer- or nanometer-scale thickness. The thermal resistance of the interface between dielectric thin films and their silicon substrate was also obtained. The obtained thermal conductivity of silicon dioxide film is 1.23 W/（m.K）, and the interface thermal resistance between silicon dioxide film and substrate is 2.35×10^-8 m^2.K/W. The thermal conductivity and interface thermal resistance of silicon nitride film are 1.07 W/（m.K） and 3.69×10^-8 m^2.K/W, respectively. The experimental results are consistent with reported data. 相似文献
2.
Amorphous InGaZnO (a-IGZO) films were deposited on the corning eagle XG (EXG) glass substrates using magnetron sputtering
method. The structure, surface morphology, electrical and optical properties of these films were investigated by X-ray diffraction
(XRD), scanning electron microscopy (SEM), semiconductor parameter analyzer and spectrophotometry, respectively. The influence
of oxygen flow on the electrical properties of IGZO thin films was studied, showing that increasing oxygen flow changes the
resistivity with six orders of magnitude. The contact resistance of ITO/IGZO is 7.35×10−2 Ω·cm2, which suggests that a good ohmic contact exists between In2O3: Sn (ITO) and IGZO film. 相似文献
3.
Pakistani wheat varieties are grown over a wide agro-climatic range and as such are anticipated to exhibit yield and quality differences. It is therefore necessary to investigate the nutritional status of wheat varieties in terms of biochemical and physiochemical characteristics available for food and nutritional purposes in Pakistan. The result shows that wheat grains of different varieties contain a net protein level of 9.15%～10.27%, 2.15%～2.55% total fats, 1.72%～1.85% dietary fibers,77.65×10^-6～84.25×10^-6 of potassium and 7.70× 10 6～35.90× 10^-6 of sodium ions concentration, 0.24× 10^-6～0.84× 10^-6 of phosphorus, 1.44%～2.10% ash, 31.108～43.602 g of thousand grain mass （TGM） and 8.38%～9.67% moisture contents. This study is significant in providing an opportunity to explore the available wheat varieties and to further improve their nutritional excellence and also essential for setting nutritional regulations for domestic and export purposes. 相似文献
4.
Luciferase from firefly lantern extract was immobilized on CNBr-activated Sepharose 4B. The kinetic properties of immobilized
luciferase were extensively studied. TheK
m′ for D-luciferin is 11.9 μmol/L, the optimum pH and temperature for Sepharose-bound enzyme were 7.8 and 25°C respectively.
A luminescence fiber optic biosensor, making use of immobilized crude luciferase, was developed for assay of ATP. The peak
light intensity was linear with respect to ATP concentration in range of 10−9–10−5 mol/L. A biological application was also demonstrated with the determination of serum ATP from rats bred in low versus normal
oxygen environments. 相似文献
5.
Well-cubic perovskite lanthanum aluminate (LaAlO3) film on (110) silicon substrate was fabricated by sol-gel method with corresponding inorganic salts. Lanthanum acetate and
aluminum acetate glacial acetic acid solutions were prepared via ligand exchange starting from lanthanum nitrate hexahydrate
and aluminum nitrate hexahydrate after being refluxed. (CH3CO)2O removed nitrates and the crystallized H2O completely, acetylacetone (AcAc) was partially bidentated with metallic ion of the metallic acetates and formed La(OAc)3−x
(AcAc)
x
which were hydrolyzed into La(AcAc)3−x(OH)
x
by adding 10 ml 0.4% methyl cellulose (MCL) solution. The La(AcAc)3−x
(OH)
x
, polymerizing and combining with MCL, formed the LaAlO3 sol precursor with heteropolymeric structure and formed film easily. The epitaxial LaAlO3 film on Si(110) substrate was crystallized after being annealed in thermal annealing furnace for 650–750 °C/30 min. The morphologies
and microstructures were characterized. The refractive index of the LAO film was 1.942 to 2.007; the dielectric constant and
the dissipation factors were estimated to be 23–26 and 2.1×10−4−2.4×10−4 respectively.
Project (No. 2002CB613305) supported by the National Basic Research Program (973) of China 相似文献
6.
In this study aimed to evaluate the pollution extent of metals and nonmetals inside and outside the ferrosilicon production factory in Edfu, Aswan, Egypt, raw materials (quartz, cokes, iron oxides), ferrosilicon alloy, silica fume, dust and suspended dust (at different sites) samples were collected from the factory, and fallen dust samples were collected from outside the factory, horizontally (at different sites and different distance and directions) and vertically (at different floors in the selected buildings). Gravimetric methods, X-ray fluorescence (XRF), flame photometer, wide range carbon determinator and atomic absorption spectroscopy tools were used for elements determination. The results indicating that the fallen dust and its element contents on southern factory walls being higher than those on eastern factory walls may be due to the nature of the dusts and effects of wind force and wind direction. Fallen dust levels in different regions outside the factory were found to be affected by the distance, direction and floors. The nature of dust samples was affected by gravity and the suspended dust in different factory units depended on the work capacity and method of handling materials by personnel in different production units. Silica fume was a complicated problem, had dangerous effect against the workers' health, and was characterized by high concentrations of SiO2(90.6%～93.6%) and heavy metals (Mn, 420.6×10-6～520.3×10-6; Fe, 2354×10-6～2685×10-6; Co, 80.7×10-6～101.6×10 6 and Ni,5.3× 10-6～6.05× 10-6). The TSP (Total Suspended Particulate) levels in all factory units were higher than the recommended air quality value (70 μg/m3) under Egyptian law. The effect of ferrosilicon factory fallen dust on the surrounding regions decreased with increasing distance between the factory and these regions. The suspended dust samples in the factory units and their components greatly exceeded national and international standards, so health and environmental criteria must be enforced on these units. 相似文献
7.
Shao-zhi Zhang Xiao-yi Yu Guang-ming Chen 《Journal of Zhejiang University. Science. B》2012,13(3):213-220
Osteochondral allografting has been proved to be a useful method to treat diseased or damaged areas of joint surfaces. Operational
long-term stocks of grafts which supply a buffer between procurement and utilization would contribute to the commercialization
or industrialization of this technology. Vitrification has been thought to be a promising method for successful preservation
of articular cartilage (AC), but high concentration cryoprotectants (CPAs) are used which may cause high cellular toxicity.
An effective way to reduce CPA toxicity is to increase CPA concentration gradually while the temperature is lowered. Understanding
the mechanism of CPA permeation at subzero temperatures is important for designing the cryopreservation protocol. In this
research, the permeation of dimethyl sulfoxide (Me2SO) in ovine AC at subzero temperatures was studied experimentally. Pretreated AC discs were exposed in Me2SO solutions for different time (0, 5, 15, 30, 50, 80, and 120 min) at three temperature levels (−10, −20, and −30 °C). The
Me2SO concentration within the tissue was determined by ultraviolet (UV) spectrophotometry. The diffusion coefficients were estimated
to be 0.85×10−6, 0.48×10−6, and 0.27×10−6 cm2/s at −10, −20, and −30 °C, respectively, and the corresponding activation energy was 29.23 kJ/mol. Numerical simulation was
performed to compare two Me2SO addition protocols, and the results demonstrated that the total loading duration could be effectively reduced with the
knowledge of permeation kinetics. 相似文献
8.
1, 10-Phenanthroline (phen) was tested as a complexing agent for on-line preconcentration of iron on RP-C18 material in a microcolumn with flow injection coupled with flame atomic absorption spectrometer (FI-FAAS). The on-line formed
Fe(II)-phen complexes were adsorbed on the C18 sorbent material. Various parameters affecting the on-line Fe(II)-phen complex formation and its subsequent adsorption in
the microcolumn as well as its elution into the nebulizer of AAS were optimized. A 2.5×10−3 mol/L phen in 2% through the microcolumn for 30 s. The adsorbed Fe(II)-phen complexes in the microcolumn were eluted with
ethanol in 10 s into the nebulizer of AAS. Ascorbic acid (5×10−4 mol/L) was added to the sample solution for the reduction of Fe(III) to Fe(II). A good precision (RSD=1.1%,n=10), high enrichment factor (19) and sample throughput (90 h−1) with detection limit (3σ) of 3 μg/L were obtained. The method was applied on standard reference materials (i. e. mussel
and tomato leaves,) for iron determination and yielded results agreeing well with certified values.
Project supported by the Zhejiang Provincial Natural Science Foundation of China and Zhejiang Environmental Protection Foundation
From Pakistan Institute of Nuclear Science & Technology, Islamabad, Pakistan and now ZJ University, Ph. D. student. 相似文献
9.
In this paper, the author proves that theL
p-boundedness of the Marcinkiewicz integral μΩ on product domainsR
n×Rm; for Ω∈(1)∩(5) improves the result of Chen et al. (2000).
Project supported by Major Project of NSFC (No.19631080) and NSF of Zhejiang province (No. RC97017). 相似文献
10.
Objective: To observe the effect of Yangxueqingnao particles on rat vascular smooth muscle cell (VSMC) proliferation induced
by lysophosphatidic acid (LPA). Methods: The amount of3H-TdR (3H-thymidine) admixed in cultured rat VSMC was measured and mitogen-activated protein kinase (MAPK) activity and lipid peroxidation
end product malondialdehyde (MDA) content of the VSMC were assayed. Results: 1×10−9, 1×10−8, 1×10−7 mol/L LPA in a concentration dependent manner, induced the amount of3H-TdR admixed, MAP kinase activity, and MDA content of the cultured rat VSMC to increase. However, 5%, 10%, and 15% Yangxueqingnao
serum preincubation resulted in a decrease of 23.0%, 42.0%, and 52.0% (P<0.01) respectively in the amount of3H-TdR admixed, a decline in VSMC MAP kinase activity of 13.9% (P<0.05), 29.6% (P<0.01), and 48.9% (P<0.01) respectively, and also, a decrease in MDA content of VSMC of 19.4%, 24.7%, and 43.2% (P<0.01) respectively, in the 1×10−7 mol/L LPA-treated VSMC. Conclusions: LPA activates the proliferation and lipid peroxidation of VSMC in a concentration dependent
manner. The LPA-induced VSMC proliferation is related to the activity of MAP kinases, enzymes involved in an intracellular
signalling pathway. The results of the present study showed that Yangxueqingnao particles can effectively inhibit LPA-induced
VSMC proliferation, MAP kinase activation, and reduce lipid peroxidative lesion.
Project (No. 491010-W50339) supported by Chinese Traditional Medicine Administration Bureau of Zhejiang Province, China 相似文献
11.
1 Introduction Ahugeamountofliteratureexistsonthestudyofi dentifyingtracemetalionsbymeansofspectropho tometry[1 3] ,fluorimetry[4 6 ] aswellas polarogra phy[7 9] ,whichhaveactiononlocatingtheendpointoftheindicatingreaction .Howeverbothspectropho tometryandfluorimetryareeasytobeinterferedbycolororprecipitation ,whilepolarographyhasanissueofmercurypollution .Thecatalyzingkineticanalysishasthecharacteristicsofhighsensitivityandspeedi ness.Oscillographicpotentiometryisasimpleintu itionisticanal… 相似文献
12.
INTRODUCTION With the development of modern electronics,there is a growing trend of designing a low-voltagehigh precision current reference in many mixed-signaland analog circuits such as data converters (Mehr andSinger, 2000; Oh et al., 2004), oscillators and PLLs(Razavi, 2001; Banba and Shiga, 1999). Low-costreasons need the reference to be realized in simplestandard CMOS logic process technology, withoutresorting to the use of BiCMOS process and specialdevices such as floating-g… 相似文献
13.
INTRODUCTION Nitrogen oxide (NOx) is one of the main air pol- lutants found in the flue gases from chemical and power plants belching acid rain and photochemical smog. Over 90 percent of all man-made nitrogen ox- ides that enter our atmosphere are produced by the combustion of various fuels. Compared with the ad- vanced stage of SO2 gas removal technologies devel- opment, the removal of NOx gases is still in the initial stages of development as roughly 90 to 95 percent of NOx emitted i… 相似文献
14.
Jin Jin-sheng 《浙江大学学报(A卷英文版)》2001,2(4):384-387
The surface morphology and growth mechanism of an aluminum film system deposited on silicone oil surfaces by a vapor depositing
method was investigated by scanning electron microscopy. It was found that the perpendicular fluctuation of the film's bottom
surface was more remarkable than that of the film's top surface. Near the joint between the film on the silicone oil substrate
and the film on the silicon wafer surface on which the silicone oil substrate rested, was a naturally formed anomalous wedge-shaped
wrinkly structure with slopes of 10−4–10−5 rad, whose growth mechanism could be interpreted under the assumption of the thermal expansion behavior of the liquid substrates.
Project supported by NSFC (No. 19874016) and the Special Fund of Zhejiang Provincial Natural Science Foundation for Young
Scientists (Grant No. 1997RC9603). 相似文献
15.
46 inbred NIH mice were infected by chloroquine resistant strain of Plasmodium yoelii. The ultrastructure changes were observed
under the administration of ketotifen(10mg·kg−1·d−1) and chloroquine(10mg·kg−1·d−1) combination and one after another respectively. The effect of taking ketotifen and chloroquine combination showed that parasites
died rapidly with a few of intermittent membranes and vacuoles. The effect of taking two kinds of drugs one after another
showed that there were exceedingly rich membranes, concentric arrangement structures similar to rough endo-reticulum and conspiciously
blocking of the formation of food vacuoles. 相似文献
16.
INTRODUCTION Motor vehicles continue to be the dominant source of air pollution, despite tremendous advances in engine technology and pollution control. Vehicles are significant sources of CO, HC, and PM and comprise one of the most important sources of NOx, which along with HC, are the essential precursors of ground-level ozone. In view of emissions harm to human health, major efforts to control them have been made, both through improved emission control technologies and through gasol… 相似文献
17.
Some laboratory diffusion tests were conducted with diffusion device to determine the diffusion coefficient of Cr(Ⅵ) ion passing through Dalian red clay samples. The concentrations of Cr(Ⅵ) at different places of the samples were then measured spectrophotometrically after a standing time of 1 000 d. A one-dimensional solute transport equation was used to simulate the transport of Cr(Ⅵ) through clay samples. Back-calculation of diffusion coefficient of Cr(Ⅵ) was made with finite difference method. Parametric analysis was conducted to simulate variations in soil dry density, temperature, pH and standing time. The results show that the method used in this paper is simple and effective. The diffusion coefficient of Cr(Ⅵ) in Dalian red clay varies from 1.50×10-7 cm2/s to 2.08×10-7 cm2/s. After 1 000 d diffusion, the concentration of the source solution drops down to 1.27 mg/L from 62.5 mg/L, and the diffusion distance is only 3.5 cm. Under the assumption that diffusion coefficient is constant, the diffusion effect becomes more obvious with lower density, lower temperature, higher pH value, and much more time. 相似文献
18.
INTRODUCTION Over the recent decades extensive research on atmospheric particles in urban environments was carried out. Most of the following papers refer to their authors’ contribution to air pollution and the effects on human health (Dzubay and Mamane, 1989; van Borm et al., 1989; 1990; Rojas et al., 1990; Paoletti et al., 1991; 1999; Al-Rajhi et al., 1996; McMurry et al., 1996; Querol et al., 1996; BéruBé et al., 1997; Esteve et al., 1997; Harrison et al., 1997; Zou and Hooper… 相似文献
19.
LU Bao - qi 《上海大学学报(英文版)》2005,9(4):365-368
Infrared （IR） absorption spectra and X-ray powder diffraction （XRD） patterrns of sexpenfine cat＇s eye from Sichuan Province have been investigated, and infrared absorption bands of the serpentine have been assigned in this paper. The results indicate that the bands near 3 600 - 3 700 cm^-1 belong to the stretching absorption band VOH, the bands in 948 - 1 100 cm^-1 axe assigned to the stretching vibraling band Usvo, and the bands at 600 570 and 440 cm^-1 respectively belong to the bending vibration band VOH, δMg-O and δSi-O. The serpentine cat＇ s eye includes two types： chrysotile and antigorite. Chrysotile has a sharp and intensive band at 3 688 cm^-1 and a weak band at 3 643 cm^-1 , while antigorite has only one intensive band in the region. At vibration band VSi-O, chrysotile and antigorite have a similar feature at 1 071 cm^-1, but the band at 980 cm^-1 in anfigorite has been split into two bands in chrysotile - a strong one at 1 027 cm^-1 and a weak one at 949 cm^-1. In addition, antigorite has a characteristic bending vibrating band δMg-O at 570 cm^-1. Based on the analysis of the feature of crystal structure, their IR differences axe well explained. 相似文献
20.
1 Ｉｎｔｒｏｄｕｃｔｉｏｎ Ｔｈｅｃｈｅｍｉｃａｌｅｆｆｅｃｔｓｏｆｕｌｔｒａｓｏｕｎｄａｒｅｄｕｅｔｏｈｉｇｈｐｒｅｓｓｕｒｅｐｒｏｄｕｃｅｄｄｕｒｉｎｇｖｉｏｌｅｎｔｃｏｌｌａｐｓｅｏｆｃａｖｉｔａｔｉｏｎｂｕｂｂｌｅｓ.Ｔｈｅｒｅａｃｔｉｏｎｓｄｏｎｏｔｔａｋｅ ｐｌａｃｅｈｏｍｏｇｅ ｎｅｏｕｓｌｙｉｎｔｈｅｓｏｌｕｔｉｏｎｂｕｔｉｎ”ｈｏｔｓｐｏｔｓ”ｗｈｅｒｅｃａｖｉ ｔａｔｉｏｎｂｕｂｂｌｅｓｐｕｌｓａｔｅｏｒｃｏｌｌａｐｓｅ .Ｄｕｒｉｎｇｔｈｅａｄｉａｂａｔ ｉｃｃｏｍｐｒｅｓｓｉｏ… 相似文献