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1.
以间歇碳化法制备纳米碳酸钙的工艺为基础,以压电超声波辅助合成为方法,以实现工业化生产优质的纳米碳酸钙为目的,确定了超声辐照下纳米碳酸钙的合成反应罐结构及合成装置系统的设计,并探讨了超声波辐照下工艺过程各影响因素与纳米碳酸钙粒径的关系。图示了反应体系的传热、传质效果及与粒径的关系。结果表明,影响压电超声在碳化法合成纳米碳酸钙的粒径主要因素有料浆初始温度、C a(O H )2乳液浓度、C O 2的流量。在自制的装置中,制备出10~30nm 优质的纳米碳酸钙产品,为纳米碳酸钙粉料的生产提供了另种方法。  相似文献   

2.
研究了双峰中密度聚乙烯(BMDPE)与纳米碳酸钙不同配比复合物的流变行为与力学性能.讨论了复合物的组成、剪切应力和剪切速率以及温度对熔体粘度和膨胀比的影响,测定了不同配比熔体的非牛顿指数(n)、熔体流动速率(MFR)、粘流活化能以及习用屈服应力,断裂应力和断裂伸长率,用扫描电镜观察了纳米碳酸钙在复合材料中的分散情况.结果发现:纳米碳酸钙可以均匀地分散在BMDPE中,少量的纳米碳酸钙就可以明显提高材料的力学性能,在较高的剪切速率下还可以改善材料的加工性能.  相似文献   

3.
以纳米碳酸钙为模板,通过无皂乳液包覆法制备出以纳米碳酸钙为核聚合物为壳的复合颗粒,再通过酸溶合成聚合物空心球,分析制备过程的机理特别是对pH值的影响,  相似文献   

4.
用旋转反应器合成纳米碳酸钙的研究   总被引:1,自引:0,他引:1  
以自行研制的打孔碟片为填料,利用pH计及电导率仅确定氢氧化钙在旋转反应器中的碳化时间,用超滤膜分离氢氧化钙与碳酸钙;探讨了气体浓度、转速、分散剂等操作条件对碳化过程的影响,结果表明:氢氧化钙与二氧化碳反应生成纳米碳酸钙的过程中,气体浓度、转速、分散剂影响反应时间、产品粒度及粒度分布;利用旋转反应器制备出平均体积当量直径为30—40cm,粒度分布很窄的菱形纳米碳酸钙,而且在碳化过程中,碳酸钙不易在碟片填料中结垢。  相似文献   

5.
本文利用洋葱内表面模板法制备了草酸钙和碳酸钙纳米材料.产物草酸钙形状为纳米棒,宽约100nm,长约1~2μm,组装成像鸟巢一样的结构.碳酸钙样品呈现均匀规则的球型,其直径约为1μm,球面不平滑,是由粒径约50nm的粒子组成,粒子与粒子直径有大量的缝隙.  相似文献   

6.
碳酸钙晶须的制备进展   总被引:1,自引:0,他引:1  
文中对碳酸钙晶须的成核生长机理进行了简要的理论分析,阐述了碳酸钙晶须的制备研究进展,比较了典型方法合成碳酸钙晶须的异同,并对未来碳酸钙制备技术的发展方向提出了建议。  相似文献   

7.
以十六烷基三甲基溴化铵(CTAB)为有机模板,加入到丙三醇和水的混合溶液中制备碳酸钙并在其母液中进一步合成羟基锡酸锌包覆碳酸钙.通过XRD,SEM,TG-DSC分别对产物的晶型、形貌、热解行为进行了分析,并研究了CTAB浓度对碳酸钙的形貌和晶体结构的影响.结果表明:碳酸钙为枝状文石型碳酸钙,羟基锡酸锌较好的包覆在枝状碳酸钙表面,当CTAB质量浓度为2.2 g/L时,枝状晶体形态最好.  相似文献   

8.
L-组氨酸作为碳酸钙晶体生长调节剂,在水热条件下合成了碳酸钙晶体,用粉末XRD衍射方法和红外光谱对合成的晶体进行了表征,用扫描电镜对生成的碳酸钙晶体形貌进行了研究,研究结果发现,在反应条件下合成的是纯的文石晶体。  相似文献   

9.
采用碳酸钙与少量氧化镁对含铬废水进行除铬处理。实验考察了碳酸钙及氧化镁的用量、搅拌时间、温度及pH值对处理结果的影响,探讨了碳酸钙处理含铬废水的机理。结果表明,在pH为2-3范围内,吸附处理剂用量:碳酸钙约9g.L-1和氧化镁约0.09g.L-1,搅拌时间30min,常温下操作,铬的去除率可达99%以上。对含铬在10mg.L-1左右的废水,一次处理即可达标排放。使用过的碳酸钙与氧化镁回收后,可再次用于处理含铬废水。  相似文献   

10.
选取HX-1500碳酸钙和PVC活性碳酸钙应用在PVC扣板生产中,考察了不同种类碳酸钙对扣板生产过程中的加工性能和制品颜色的影响,分析了碳酸钙种类对PVC扣板的横向和纵向拉伸、弯曲、冲击强度等力学性能的影响。结果表明,在相同的配方条件下,碳酸钙目数增加,熔体挤出性能变差,加工电流增大,制品略微变黄;但冲击强度有非常明显的改善。  相似文献   

11.
《海外英语》2007,(5):44-45
It is worthy of noting that, whilst Crookston Castle witnessed the earlier and happier portion of Mary's variegated life,  相似文献   

12.
《海外英语》2007,(4):36
There are numbers of crossroads on our long and unpredictable life journey where we totally have no idea about which direction to choose. No matter what our decision is, we should not turn back, but face the music and go ahead instead. I am this kind of girl who always does try without regretting, one example is how I dealt with my love.  相似文献   

13.
王菲 《华章》2007,(12):273-273
Migration occurs behind a variety of reasons and has a great effect on the whole world. People may migrate in order to improve their economic situation, or in order to escape civil strife, persecution, and environmental disasters. The impact of migration is complex, bringing both benefits anddisadvantages. This paper briefly talks about the causes of migration, the allocation of benefits, and the ways in which individual countries and the international community deal with this important subject.  相似文献   

14.
裴水妹 《华章》2007,(11):196
Sister Carrie is one of the most controversial characters in American literature.Thought as a "fallen woman" firstly,she was defined as a "new woman" by some critics later. However, by digging into the motivaton behind the whole process of Carrie's "success", the relationship between Carrie and her creator (the author), the social conditions of then American, it can be found that Carrie has never been free-standing on her thought and she has never found her real-sdf even after becoming a famous actress. In a society dominated by mass consumerism Carrie is only an adherent of her own desires. She also is a representative of all those country girls flooded into cities, a symbol and a sacrifice of the urbanization of America in a time countryside was overcome by cities.  相似文献   

15.
16.
1.IntroductionOne-cyclecontrolmethod,whichwasproposedaboutonedecadeago[1],hasbecomeanattractivemethodinspecialfieldssuchaspowerfactorcorrection[2-6],switchingamplifiers[7,8],etc.Themainideaofthiscontrollerisbasedonintegrationofdiodevoltageinone-cycleandforcesittobeexactlyequaltothereferencevalue.Themainadvantageofthiscontrollerisitsrealtimeabilitytorejectthevariationofinputvoltage[1].Despitethisgreatability,ithasnogoodperformancesinrejectingofloaddisturbanceandfollowingreferencecommands.Espec…  相似文献   

17.
Today, Sunday morning, I sit thinking and typing at my computer. My thoughts are in my homeland, India and my body is in China. The body is here and mind there for a good reason. Mr. Hu is president and I am resident and both are in each other's countries (what a difference the absence of one small letter makes!). Mr. Hu will return in a few days and I will stay on longer.  相似文献   

18.
STORIES     
正A One day a pig went to the stable(马棚)to see his good friend,an oldhorse,and was going to stay there forthenight.Night came and it was time forsleep.The pig went into the straw heap(稻草堆)and lay comfortably.A longtime passed,but the horse was stillstanding there and did not move.Thepig asked the horse why he did not go tosleep."Standing like this is the begin-ning ofsleeping,"answered the horse.  相似文献   

19.
正1.Any fool can count the seeds in an apple.Only God can count all the apples in one seed.2.Happy families are all alike;every unhappy family is unhappy in its own way.3.Memories are the key not to the past,but to the future.4.Sometimes in the dark you see what you want to see.5.There is a great difference between  相似文献   

20.
正Scope and Policy The Journal of Chongqing University-English Edition(JCQU-E)is a peerreviewed journal publishing research articles in multiple disciplines of science and technology,covering civil and environmental engineering,chemical engineering,biotechnology,mechanical and electrical engineering,computer and data processing,mining,metallurgy,materials science,and interdisciplines thereof.  相似文献   

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