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1.
超临界流体萃取温郁金中的挥发油   总被引:11,自引:0,他引:11  
颜继忠  童胜强  陈钢 《科技通报》2004,20(4):355-358
目的 采用超临界流体萃取温郁金中的挥发油.方法 采用正交试验对萃取条件进行了优化.结果 确定了最佳萃取条件:萃取时间90min、CO2动态流量4kg/h、萃取压力20MPa、萃取温度55℃;并用GC/MS确定了挥发油中的10种主要成分.结论 与水蒸汽蒸馏法相比较,超临界萃取法具有萃取率高、耗时少等优点.  相似文献   

2.
本试验为确定分离猪胰岛的最佳胶原酶浓度,以屠宰猪胰腺为试验材料进行猪胰岛分离纯化研究。结果表明,猪胰岛获取量与不同浓度胶原酶1.0 mg/ml、1.5 mg/ml、2.0 mg/ml各组间均差异显著(P0.05);在相同的消化时间(15 min)条件下,猪胰岛分离1758±125个/g,纯化后1485±119个/g,纯度为84%存活率为92%。由此可知,屠宰猪胰岛分离的最佳胶原酶浓度为1.5mg/ml,而最佳消耗时间为15 min。  相似文献   

3.
利用单因素试验筛选培养基碳氮源及氮源分别为玉米粉及豆柏粉,正交试验确定最佳培养时间为2天时,最佳液体发酵条件转速200r/min,温度30℃,装液量为50ml∕250ml,起始p H5.0。  相似文献   

4.
目的用正交试验法优选砂生槐提取工艺。方法以浸膏得率、苦参碱提取率为评价指标,选择酸水浓度(ml/L)、加酸水量(倍)、提取时间(h)、为考察因素,利用正交试验L9(33)确定酸水提取砂生槐工艺.结果最佳提取工艺条件为药材加6倍量、2%酸水、提起2次、每次回流1小时。结论在正交试验前,曾将酸水提法与不同浓度乙醇提取苦参碱作比较,尽管醇提取率比酸水提的要高,但考虑到大规模提取时降低成本的问题,本实验选用了不同浓度的酸水进行正交试验,为下一步的大规模分离提取提供了理论依据。  相似文献   

5.
本实验采用高速逆流色谱法对何首乌活性成分二苯乙烯苷进行分离。色谱条件为:正已烷-乙酸乙酯-乙醇-水(1:48:1:48)流速2.0ml/min,检测波长280nm。该方法简便、快捷适合分离何首乌中的二苯乙烯苷。  相似文献   

6.
以无水乙醇和无水乙醛为原料,以无水氯化氢为催化剂制备乙醛缩二乙醇.利用正交试验的方法找出优化方案.通过单因素实验和正交实验确定出最佳反应条件为:无水乙醇与无水乙醛摩比为2.4:1.0,温度:30C~50C.硅胶用量为34g,反应时间 55min,通入新蒸的氯化氢13min,产率可以到90%以上.  相似文献   

7.
采用单因素和正交实验设计,优化花生壳中白藜芦醇的超声波辅助浸提工艺,最佳工艺条件为:料液比为1∶25、乙醇浓度为50%、超声时间为35min、超声温度为30℃,为花生壳的利用提供了新途径。  相似文献   

8.
连翘提取物制备工艺以连翘酯苷收率为指标,进行L9(3^4)正交试验对乙醇浓度、乙醇用量、提取时间和提取次数进行了优选,确定了最佳的回流提取条件。此外所建HPLC含量测定方法操作简便、重复性好、精密度高、回收率稳定、结果准确可靠,可用于连翘提取物的质量控制。  相似文献   

9.
目的:建立灵敏度高、操作简单的高效液相色谱法测定熟肉制品中柠檬黄、日落黄、胭脂红、诱惑红等合成色素。方法样品经涡旋离心等提取,得出最佳色谱条件,注入高效液相色谱仪进行分离。结果在选定的分离条件下4种色素在0.0-60.0ug/ml范围内线性关系良好,相关系数均≥0.9995。准确度试验,回收率在89.0%-109.5%。结论方法简单易操作,应用于实际样品的测定,结果满意。  相似文献   

10.
以聚乙二醇为固定相的强极性毛细柱,H2为载气,利用FID检测器气相色谱法使1,4-丁炔二醇和二次分成的组分分离,并以色谱柱的分离度作为分离效率的指标,研究柱温及载气流速对分离度的影响,最后确定最佳的操作条件。在此基础上以1,4丁二醇为内标物,采用内标法对1,4-丁炔二醇组分的定量。该方法快速,简单,可在1,4丁二醇的工业生产中作为一种分析方法来应用。  相似文献   

11.
Aresearch group led by Prof. ZHAI Qiwei from the Institute for Nutritional Sciences under the CAS Shanghai Institutes for Biological Sciences has discovered that even relatively low doses of resveratrol--a chemical found in the skins of red grapes and in red wine--can improve the sensitivity of mice to the hormone insulin, according to a report in the October,2007 issue of Cell Metabolism. As insulin resistance is often characterized as the most critical factor contributing to the development of Type 2 diabetes, the findings“provide a potential new therapeutic approach for preventing or treating” both conditions, the researchers said.  相似文献   

12.
This study examined how students who had no prior experience with videoconferencing would react to the use of videoconferencing as an instructional medium. Students enrolled in seven different courses completed a questionnaire at the beginning of the semester and again at the end of the semester. Students at the origination and remote sites did not differ in their reactions toward videoconferencing but there was a significant difference for gender. Women reacted less favorably to videoconferencing. Compared to the beginning of the semester, students reported significantly less positive attitudes toward taking a course through videoconferencing at the end of the semester. There were no significant differences in students' attitudes toward videoconferencing across courses at the beginning of the semester but there were significant differences across the courses at the end of the semester. The results suggest the need for better preparation for both students and instructors.  相似文献   

13.
Ajoint study by Prof. ZHANG Zhibin from the CAS Institute of Zoology and his co-workers from Norway, US and Swiss have indicated that historical outbreaks of migratory locusts in China were associated with cold spells, suggesting that China's projected climate warming could decrease the pest's numbers. The study was published in Proceedings of theNational Academy of Sciences on 17 September, 2007.  相似文献   

14.
A computer-mediated group is a complex entity whose members exchange many types of information via multiple means of communication in pursuit of goals specific to their environment. Over time, they coordinate technical features of media with locally enacted use to achieve a viable working arrangement. To explore this complex interaction, a case study is presented of the social networks of interactions and media use among members of a class of computer-supported distance learners. Results show how group structures associated with project teams dominated who communicated with whom, about what, and via which media over the term, and how media came to occupy their own communication niches: Webboard for diffuse class-wide communication; Internet Relay Chat more to named others but still for general communication across the class; and e-mail primarily for intrateam communication. Face-to-face interaction, occurring only during a short on-campus session, appears to have had a catalytic effect on social and emotional exchanges. Results suggest the need to structure exchanges to balance class-wide sharing of ideas with subgroup interactions that facilitate project completion, and to provide media that support these two modes of interaction.  相似文献   

15.
Active biological molecules and functional structures can be fabricated into a bio-mimetic system by using molecular assembly method. Such materials can be used for the drug delivery, disease diagnosis and therapy, and new nanodevice construction.  相似文献   

16.
CAS should stick to the principle of rendering service to, and giving impetus for, the development of China's science enterprise by making S&T innovations, said CAS President LU Yongxiang. The CAS president made the remarks in a recent talk to communicate the gist of the winter session of the Party's Leading-member Group at CAS, which was held from 7 to 11 January in Beijing.  相似文献   

17.
With great care, Dr. ZHOU Zhonghe takes out a package wrapped by cotton tissue from a drawer and says: "This is the gem of our collections: the fossil of a bird that lived 125 million years ago!" Then, pointing at a tiny mound, he explains: "Look, this is the claw and that is the head. It was in the egg shell and ready to hatch ... The species fell into a family of waterside inhabitants."  相似文献   

18.
Electronic data interchange (EDI) provides means for interorganizational communication, creates network externalities, requires an advanced information technology (IT) infrastructure, and relies on standards. In the diffusion of such innovations, institutional involvement is imperative. Such institutions contain governmental agencies, national and global standardization organizations, local government, and nonprofit private organizations like industry associations. The last type of organizations we call intermediating institutions. They intermediate or coordinate ("inscribe") the activities of a group of would-be adopters. Unfortunately, little is known of how these organizations shape the EDI diffusion trajectory. In this article we examine one specific type of intermediating organizations?industry associations?and how they advanced the EDI diffusion process in the grocery sectors of Hong Kong, Denmark and Finland. We identify six institutional measures, placed into a matrix formed by the mode of involvement (influence vs. regulation) and the type of diffusion force (supply push vs. demand pull), that can be mobilized to further the EDI diffusion. Industry associations were found to be active users of all these measures to varying degrees. Their role was critical especially in knowledge building, knowledge deployment, and standard setting. Furthermore, institutional involvement varied due to policy and cultural contingencies and power dependencies.  相似文献   

19.
This essay focuses on universal service and the Internet as means to support social and political participation. The emphasis on access to telecommunications systems in conventional approaches to universal service is contrasted with access to content. A model of the information environment is described that accounts for the roles of content and conduit, both of which are necessary conditions to achieve true access. A method is outlined for employing information indicators to observe or measure the information environment.  相似文献   

20.
The increasing prospects of digital piracy has prompted the perceived need by electronic publishers to adopt technical systems of protection, and governments to reform their copyright laws. This article is a preliminary study of the management of intellectual property by electronic publishers, defined as those involved in the production of online databases, and CD-ROMs. It focuses on three main issues: (1) how electronic publishers view the increasing threat of piracy; (2) the methods of protection employed to protect intellectual property in digital format; and (3) the importance of technological protection of intellectual property in electronic publications. The analysis is based on a sample of 23 UK electronic publishers. The interviews revealed an interesting assortment of protection methods and did not show that technological protection was a preferred way. Instead, the means of protection, in addition to copyright law, comprised niche markets, pricing, trust, bad publicity, and nontechnical and technical means.  相似文献   

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