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In2O3 nanoparticles were prepared from or with different indium salts by chemical precipitation under the conditions of various pH values. The crystal structure and ceramic microstructure of the samples were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results show that the mean grain size of In2O3 is less than 100 nm, and their particle homogeneity and dispersibility are satisfactory. The gas sensitivity defined as Ra/Rg was detected in a static system. The results show that the sensors made by as-prepared nanoparticles has high sensitivity to many gases such as alcohol, HCHO, NH3 , et al. The response time is less than 20 s and the recovery time is lower than 30 s.  相似文献   
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本文以乙醚作为溶剂兼作保护剂,通过铜盐与金属铜的化学反应制备了溴化物亚铜气敏材料,并用X-射线衍射对所合成样品粉末的晶体结构和尺寸形貌进行了表征;用静态配气法测试了其气敏性能.结果显示用该法所合成的样品为立方型溴化亚铜,其粒径约为1μm.气敏测试结果表明,该元件在常温下对氨气具有较高的灵敏度,检测限可达5ppm氨气灵敏度与浓度呈较好的双对数线性关系,且具有较好的选择性,对乙醇、异丁烷、三乙醇胺、一氧化碳等均不敏感.  相似文献   
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针对我校材料专业实验教学课时大幅缩减的教学现状,从重整实验化学教材、精选实验内容入手,保障实验教学目标。注重学生动手能力、观察能力、以及科学潜质的培养,借助网络教学平台,实现教学内容互动答疑,缩短实验考评时间,保证短学期、少学时教学体系下基础化学实验课堂教学的质量。  相似文献   
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A liquefied petroleum gas (LPG) sensor with high selectivity, sensitivity and low power consumption has been developed based on indium oxide with very low resistance. Nanocrystalline In203 gas sensing materials were directly synthesized through a one-step controllable solvothermal process at 210 ℃ for 24 h, using InCI3.4H2O as the starting material, cetyltrimethyl ammonium bromide (CTAB) as additive and ethanol as the solvent. The obtained samples were characterized by X-ray diffraction (XRD), and transmission electron microscopy (TEM). The results showed that indium oxide takes on uniform cubic shape with range size of 10~30 nm and fine dispersivity. Gas sensitivity was measured in a mixing static gas. The results indicated that 3.0 V is the best working voltage of the sensor to LPG. Sensitivity is 12.6. The response-time and recovery-time are 3 s and 10 s respectively. Power consumption is only around 200 mW.  相似文献   
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