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1 液态有机物的燃烧(1)操作 :取一支尖头粉笔 ,在其尖端部位滴几滴液态有机物 (如苯、苯的同系物等 ) ,使其浸润。手拿另一端将其点燃 ,即可观察液态有机物燃烧情况。(2 )特点 :就地取材 ,操作简便 ,现象明显。适于课堂演示。启迪学生实验思维的灵活性及节俭意识。2 易燃气体的燃烧(1)实验装置 (如图 1)图 1(2 )适用范围 :适用于难溶于水 ,且易燃气体如氢气、一氧化碳、甲烷、乙烯、乙炔等。另外 ,气体其它性质实验 ,可在尖嘴处接上导管 ,后续完成。(3)特点 :简便、有效、安全。3 乙醇催化氧化为乙醛(1)仪器与试剂 :酒精灯、光亮粗铜丝。… 相似文献
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有机氟化物是药物、染料的重要中间体和化学试剂。脂肪族有机氟化物通常由相应的氯化物、溴化物或磺酸酯与氟负离子发生亲核取代反应制得,但芳卤活性较低,不易发生亲核取代反应。特别是当氟负离子作亲核试剂时,由于氟化钾(钠)在极性质子性溶剂中溶解度小,亲核能力较弱。脂肪族卤化物的氟代尚需强烈的反应条件,芳卤的氟代就更困难了。考虑到非质子极性溶剂如DMSO,DMF,HMPA等既可增加无机盐类化合物的溶解度,而且氟负离子在非质子性极性溶剂中不被溶剂化而呈裸露状态,裸露的氟负离子具有更 相似文献
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Li-hua Teng 《浙江大学学报(A卷英文版)》2008,9(9):1288-1295
Fluidized-bed reactor is a candidate for dimethyl ether （DME） synthesis from syngas because of its excellent heat removal capability. In order to improve the attrition resistance of catalyst, an amount of silica sol as binder was added to the catalyst composed of methanol synthesis component CuO/ZnO/Al2O3 and methanol dehydration component HZSM-5, which was prepared by coprecipitation and shaped by spray drying to get spherical particles. The effect of silica sol on the catalytic activity was investigated in a fixed-bed flow microreactor. Based on the experiment results, silica sol in the range of 0-20wt% had small effect on the catalytic activity. Generally, the CO conversion and DME yield decreased with the increase in concentration of silica sol, while the attrition resistance of catalysts increased with increasing silica sol, indicating that it was feasible to improve the attrition resistance without greatly sacrificing the activity of catalyst. In addition, the characterizations of catalysts were carried out using Brunauer-Emmett-Teller （BET）, X-ray powder diffraction （XRD） and temperature programmed reduction （TPR）. 相似文献
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段昌平 《数理化学习(高中版)》2008,(8):45-46
质量守恒定律是基本的重要的自然规律,也是中学生学习化学、发展能力的一种重要的逻辑思维方法.它能使人透过复杂的现象,一眼见底地看清问题的本质,从而快捷、准确、简便地解决问题.下面以四川省2007年高考理综化 相似文献
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簇模型方法是研究化学吸附的重要的量子化学方法之一,文章介绍了金属氧化物团簇的选取原则,并介绍了团簇理论在研究催化反应中的应用。 相似文献
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Para-tert-butyl phenol (p-TBP) and 2,4-di-tert-butyl phenol ( 2,4-DTBP) are wi.dely used for the preparation of antioxidants. Zeolite catalysts showed good performance for the synthesis of p-TBP and 2,4-DTBP. In this work, zeolite H-mordenite (HM) catalyst was prepared and the alkylation of phenol with tert-butyl alcohol over zeolite HM catalyst was investigated at different reaction conditions. It is found that increasing temperature enhances the selectivity to p-TBP and the optimum reaction temperature for phenol conversion is 438 K. Increasing flow rate decreases phenol conversion apparently while the selectivity to p-TBP has a little increase. The suitable tert-butyl alcohol/phenol molar ratio is 2. Lower alcohol/phenol molar ratios are beneficial to p-TBP while higher ones are helpful for producing 2,4-DTBP. 相似文献
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刘利民 《湖南师范大学教育科学学报》1996,(5)
本文将Ｃｏａｔｓ－Ｒｅｄｆｅｒｎ积分校正公式应用于ＫＣｌＯ_３与Ｆｅ_２Ｏ_３催化反应动力学研究，结果发现该公式同样适用于ＫｃｌＯ_３与Ｆｅ２_Ｏ_３催化反应，并找出了Ｆｅ_２Ｏ_３的适宜用量． 相似文献
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