| 糠酸正丁酯类香料催化合成的新方法 |
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| 引用本文： | 刘晓燕,邹贵田.糠酸正丁酯类香料催化合成的新方法[J].贵阳金筑大学学报,2001(4). |
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| 作者姓名： | 刘晓燕 邹贵田 |
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| 作者单位： | 贵阳金筑大学，贵阳金筑大学 贵州 贵阳 550005，贵州 贵阳 550005 |
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| 摘 要： | 以糠酸和正丁醇为原料,钼镍催化剂合成了糠酸酯类香料。合成糠酸酯类香料最优条件为:酸醇物质的量比1:2.5,催化剂用量为反应物质总质量的8％,反应时间3.5h,在此条件下合成了糠酸甲酯、乙酯及正丁酯。产率分别达到80％,83％,80.9％。
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| 关 键 词： | 糠酸 糠酸酯类香料 催化合成 |
Synthesis of Furoate perfumer by Salid Mo - Ni |
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| Liu Xiao - yan Zhou Gui - tian.Synthesis of Furoate perfumer by Salid Mo - Ni[J].Journal of Jinzhu University of Guiyang,2001(4). |
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| Authors: | Liu Xiao - yan Zhou Gui - tian |
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| Abstract: | furoates was syntesized by salid Mo-Ni, The aptimum conditions of the preparation of catalyst by ofr thogomal experrments were studied. The factors influemcing the yield of the esterifcation of furaic acid were diseussed. The experiment showeed that the aptimum reaction conditions were that acid: alcohel=1:2.5(molarratio), weight of catalyst=0.8g(basedan 0.1 mel furoie acid), reaction time=3. 5h. last four furaute perfumers were synthesized on these conditons The yield of title compounde is 80%, 83%,80%. |
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| Keywords: | furaic acid catalysis furoate |
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