(1) Department of Chemistry, Zhejiang University, 310027 Hangzhou, China
Abstract:
1H-NMR and13C-NMR assignments of 12-oleanene-3,11-dione (compound 1) were completely described for the first time through conventional
1D NMR and 2D shift-correlated NMR experiments using1H-1HCOSY, HMQC, HMBC techniques. Based on its NMR data, the assignments of 28-hydroxyolean-12-ene-3,11-dione (compound 2) were
partially revised.
Project (Nos. 20375036 and 20472073) supported by the National Natural Science Foundation of China