| 原位一步法合成3，5-二硝基水杨酸插层水滑石 |
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| 引用本文： | 郭军,袁邦群,胡传跃,易涛,申湘忠.原位一步法合成3，5-二硝基水杨酸插层水滑石[J].娄底师专学报,2006(6):23-26. |
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| 作者姓名： | 郭军 袁邦群 胡传跃 易涛 申湘忠 |
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| 作者单位： | 湖南人文科技学院化学与材料科学系,湖南娄底417000 |
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| 摘 要： | 采用原位一步合成法合成3，5-二硝基水杨酸插层水滑石材料，用XRD、IR对合成的样品进行表征，并与水溶液中阴离子直接交换合成法进行比较。结果表明，采用上述两种方法在控制适当的反应条件下均能制备出相应的3，5-二硝基水杨酸插层水滑石，但相比之下，原位一步合成法明显具有合成时间短，步骤简单和节约能耗等优点。
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| 关 键 词： | 3 5-二硝基水杨酸 插层水滑石 原位合戍 |
| 文章编号： | 1673-0712（2006）06-0023-04 |
| 收稿时间： | 2006-08-02 |
In Situ One-step Synthesis of 3,5-dinitrosalicylate Anion Intercalated Layered Double Hydroxides |
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| GUO Jun, YUAN Bang-qun, HU Chuan-yue, YI Tao, SHEN Xiang-zhong.In Situ One-step Synthesis of 3,5-dinitrosalicylate Anion Intercalated Layered Double Hydroxides[J].Journal of Loudi Teachers College,2006(6):23-26. |
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| Authors: | GUO Jun YUAN Bang-qun HU Chuan-yue YI Tao SHEN Xiang-zhong |
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| Abstract: | 3, 5 -dinitrosalicylate-intercalated layered double hydroxides was synthesized by in-situ one-step synthesis method for the first, and was characterized by XRD and IR. A comparison was made for the synthetic conditions between the in-situ one-step synthesis method and direct anion-exchange synthesis method. The results show that with these two methods, the 3, 5 -dini- trosalicylate-intercalated layered double hydroxide can be obtained, but in contrast, the former has the advantages of shorter synthetic time, fewer synthetic steps and lower energy consumption. |
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| Keywords: | 3 5-dinitrosalicylic acid intercalated layered double hydroxide in-situ synthesis |
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