| HPLC测定小儿喜食糖浆中柚皮苷含量 |
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| 引用本文： | 栗芬琴,刘倩,栗德蕾,张璐.HPLC测定小儿喜食糖浆中柚皮苷含量[J].商丘职业技术学院学报,2010,9(5):105-106. |
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| 作者姓名： | 栗芬琴 刘倩 栗德蕾 张璐 |
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| 作者单位： | 1. 金花企业(集团)股份有限公司西安金花制药厂,陕西,西安,710075
2. 榆林天然气化工有限公司,陕西,榆林718400 |
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| 摘 要： | 建立了HPLC法测定小儿喜食浆中柚皮苷含量测定方法.采用18烷基硅烷键合硅胶为填充剂,流动相：乙腈-水（21.5：80.5）,流速1.0ml/min,检测波长283nm.柚皮苷的线性范围为50-800μg/ml,平均回收率98.8%,精密度相对标准偏差（RSD）为0.41%,重现性RSD为1.1%,稳定性RSD值为0.32%.本方法简便、准确,可供本品质量控制.
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| 关 键 词： | 柚皮苷 高效液相色谱法 小儿喜食糖浆 |
HPLC Determination of Naringin in Citrus Fruit for Children Happily to Eat |
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| LI Fen -qin,LIU Qian,LI De-lei,ZHANG Lu.HPLC Determination of Naringin in Citrus Fruit for Children Happily to Eat[J].Journal of Shangqiu Vocational and Technical College,2010,9(5):105-106. |
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| Authors: | LI Fen -qin LIU Qian LI De-lei ZHANG Lu |
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| Institution: | 1.Xi＇an Ginwa Pharmaceutical Factory,Ginwa Enterprise(group) INC.Xi＇an 710075,China 2.Yulin Natural gas and chemical Co.,LTD Yulin 718400,China) |
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| Abstract: | Objective：To establish the quantitative method of naringin in citrus fruit for children happily to eat by using HPLC.Method：To adopt ODS-C18（150mm × 4.6mm,5μm）.Mobile phase,Acetonitrile-water（21.5：80.5） make ph：3.0 By phoric acid,flow rate at 1.0ml/min,wavelength 283nm,Result：The linear range 50-800μg/ml,the average recovery 98.8%,precision RSD 0.41%,repetition RSD 1.1%,stability RSD 0.32% 。 Conclusion：This method is accurate and reliable |
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| Keywords: | citrus fruit HPLC sirup for children happily to eat |
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