| 微波辅助四氯化锡/活性炭催化合成丁酸丁酯的研究 |
| |
| 引用本文： | 蒋海明,胡建平.微波辅助四氯化锡/活性炭催化合成丁酸丁酯的研究[J].衡阳师范学院学报,2011,32(3):69-71. |
| |
| 作者姓名： | 蒋海明 胡建平 |
| |
| 作者单位： | 湖南科技学院生命科学与化学工程系,湖南永州,425100 |
| |
| 摘 要： | 以活性炭负载四氯化锡(SnCl4/C)为催化剂,在微波辐射条件下快速合成了丁酸丁酯。实验结果表明,最佳合成条件为:以0.1 mol正丁酸为基准,醇酸摩尔比为1.3∶1,催化剂负载量20%,催化剂用量为正丁酸用量的3%,加热功率为450 W,辐射反应时间为7 min,酯化率可达86.7%。
|
| 关 键 词： | 微波辐射 丁酸丁酯 SnCl4/C |
Study on the Catalytic Synthesis of Butyl Butyrate with Stannic Chloride Supported on Active Carbon by the Aid of Microwave Irradiation |
| |
| JIANG Hai-ming,HU Jian-ping.Study on the Catalytic Synthesis of Butyl Butyrate with Stannic Chloride Supported on Active Carbon by the Aid of Microwave Irradiation[J].journal of Hengyang Normal University,2011,32(3):69-71. |
| |
| Authors: | JIANG Hai-ming HU Jian-ping |
| |
| Institution: | (Hunan University of Science and Engineering,Yongzhou Hunan 425100,China) |
| |
| Abstract: | |
| |
| Keywords: | |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
