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吸附热脱附-气相色谱/质谱联用分析卷烟主流烟气气相成分
引用本文:宋金勇,马宇平,王文领,郝辉,肖尊宏.吸附热脱附-气相色谱/质谱联用分析卷烟主流烟气气相成分[J].衡阳师范学院学报,2006,27(3):63-65.
作者姓名:宋金勇  马宇平  王文领  郝辉  肖尊宏
作者单位:许昌卷烟总厂技术中心,河南,许昌,461000
基金项目:许昌卷烟总厂科研资助项目(卷烟烟气与其感官品质相关性研究)
摘    要:用CarbotrapTM349型吸附管对国产某牌号卷烟烟气气相成分进行收集,然后利用吸附热脱附-气相色谱-质谱联用技术对烟气气相成分进行了分析。分离和鉴定了122种化合物,其中烯烃、烷烃32个、呋喃类12个、酮23个、芳香族化合物21个、含氮杂环及胺类8个、醛7个、腈7个、含硫化合物4个、酸2个、醚1个、酯2个、醇3个。并初步分析了这些化合物对卷烟安全性和感官质量的影响。

关 键 词:吸附热脱附  气质联用  剑桥滤片  烟气分析
文章编号:1673-0313(2006)03-0063-03
收稿时间:2005-09-28
修稿时间:2005年9月28日

Analysing Gas Phase Element of Cigarette Mainstream Smoke by Adsorption/Thermal Desorption
WANG Wen-ling, SONG Jin-yong , HAO Hui , LI Yan-zhou.Analysing Gas Phase Element of Cigarette Mainstream Smoke by Adsorption/Thermal Desorption[J].journal of Hengyang Normal University,2006,27(3):63-65.
Authors:WANG Wen-ling  SONG Jin-yong  HAO Hui  LI Yan-zhou
Institution:Technology Center of Xuchang Cigarette General Factory, Xuchang Henan 461000, China
Abstract:The gas phase components of one domestic cigarette mainstream smoke were collected by Carbotrap~(TM)349 tube.Then the gas components were analyzed by adsorption/thermal desorption coupled with gas chromatography/mass spectrometry(ATD-GC/MS).122 components were isolated and identified,which include 32 alkanes or alkenes,12 furans,23 ketones,21 aroma components,8 nitric heterocyclic ring components or amines,7 aldehydes,7 nitriles,4 sulfides,2 acids,1 aether and 3 alcohols.The relationship between cigarette safety,quality and 122 components were also studied.
Keywords:ATD  GC-MS  Cambridge Filter  Smoke Analysis
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