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| 氟核磁共振法定量测定甲磺酸帕珠沙星含量 | |
| 引用本文： | 吴永兰,文茜,杨明生,黄娟娟,文耀智.氟核磁共振法定量测定甲磺酸帕珠沙星含量[J].湘南学院学报,2007,28(5):53-56. |
| 作者姓名： | 吴永兰 文茜 杨明生 黄娟娟 文耀智 |
| 作者单位： | 1. 湘南学院,化学与生命科学系,湖南,郴州,423000 2. 湖南师范大学,分析测试中心,湖南,长沙,410081 3. 湖南公安高等专科学校,湖南,长沙,410006 |
| 基金项目： | 湖南省教育厅科研课题[03C010]，湖南省教育厅教育科学规划课题[05134]，湘南学院科研课题[04Y038] |
| 摘 要： | 研究了利用19F-NMR技术分析样品中甲磺酸帕珠沙星药物的含量.以三氟乙酸钠为内标(内标绝对法)进行定量分析,回收率99.2%-100.9%,标准偏差为0.004 46%-0.065 2%,变异系数小于1.459%. |
| 关 键 词： | 核磁共振 甲磺酸帕珠沙星 氟测定 |
| 文章编号： | 1672-8173（2007）05-0053-04 |
Measurement with Quantitative Determination of Fluoride in Pazufloxacin Mesilate Sample by 19F Nuclear Magnetic Resonance |
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| WU Yong-lan,WEN Qing,YANG Ming-sheng,HUANG Juan-juan,WEN Yao-zhi.Measurement with Quantitative Determination of Fluoride in Pazufloxacin Mesilate Sample by 19F Nuclear Magnetic Resonance[J].Journal of Xiangnan University,2007,28(5):53-56. | |
| Authors: | WU Yong-lan WEN Qing YANG Ming-sheng HUANG Juan-juan WEN Yao-zhi |
| Institution: | 1.Department of Chemistry and Life Science;Xiangnan University;Chenzhou 423000;China;2.Analysis and Testing Certre;Hunan Normal University;Changsha 410081;China;3.Hunan Public Security College;Changsha 410006;China |
| Abstract: | Study of quantitative analysis methods by the application of 19F-NMR internal standards to analyze fluoride in Pazufloxacin mesilate samples.The method takes trifluoroacetate natrium as its interal standards,with recoverice 99.2%-100.9% and coefficient of variation was less than 1.459%. |
| Keywords: | nuclear magnetic resonance pazufloxacin mesilate fluoride |
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