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Combined in situ micro-XRF,LIBS and SEM-EDS analysis of base metal and corrosion products for Islamic copper alloyed artefacts from Umm Qais museum,Jordan
Authors:Abeer Arafat  Maram Na’es  Vicky Kantarelou  Naseem Haddad  Anastasia Giakoumaki  Vasilike Argyropoulos  Demetrios Anglos  Andreas-Germanos Karydas
Institution:1. Royal Scientific Society (RSS), 11941 Amman, Jordan;2. Institute for Optics and Atomic Physics, Technical University of Berlin, EW 3-1, Hardenbergstr. 36, 10623 Berlin, Germany;3. X-ray Spectrometry Laboratory, Institute of Nuclear Physics, (NCSR) “Demokritos”, Aghia Paraskevi, 15310, Athens, Greece;4. Institute of Electronic Structure and Laser, Foundation for Research and Technology - Hellas (IESL-FORTH), P.O. Box 1385, 71110 Heraklion, Greece;5. Technical and Educational Institute of Athens (TEI), Department of Conservation of Antiquities and Works of Art, Ag. Spyridona, 12210 Athens, Greece;6. Department of Chemistry, University of Crete, P.O. Box 2208, 71003 Heraklion, Crete, Greece;7. Nuclear Spectrometry and Applications Laboratory, International Atomic Energy Agency (IAEA), Agency''s Laboratories Seibersdorf, A-2444, Seibersdorf, Austria
Abstract:Selected copper alloy artefacts from the collection of the Umm Qais museum at Irbid, Jordan, were studied by SEM-EDS analysis, while in situ analyses were performed by means of portable μ-XRF and LIBS spectrometers. Analysis and characterization of base metal and corrosion products of the copper alloyed artefacts were performed in relation to the environmental conditions of the display and as part of the overall assessment of the museum environment. Findings of this study are directed towards guiding a preventive conservation strategy for the copper alloyed artefacts at the Umm Qais museum.
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