共查询到20条相似文献，搜索用时 203 毫秒
1.
采用一种新型的离心喷射沉积(CSD)成形技术制备了Ti—48A1—2Mn—2Nb金属间化合物，较系统地研究了该合金的微观组织结构以及室温拉伸、压缩和断裂韧度等力学性能，探讨和研究了该合金制备过程中形成的孔隙、特殊层片状组织及对材料性能的影响规律。图像分析系统定量测试结果表明，CSD制备的金属间化合物的孔隙率在2％左右，热等静压(HIP)有效地消除了合金在喷射成形制备中产生的孔隙，致密度达99.6—99．9％。性能研究结果表明，CSD制备的Ti—48A1—2Mn—2Nb合金具有良好的室温拉伸、压缩和断裂韧度等性能，尤其是压缩性能和断裂韧度值，显示了很好的应用前景。 相似文献
2.
高一化学(必修)第24页中卤素各单质的活动性比较实验,要求使用新制备的氯水、溴水,增加了实验难度,效果不明显。本实验装置设计,可提高该实验效果。 1.实验用品及装置500mL锥形瓶,玻璃绒,玻管一支(d20mm,l70mm)青霉素瓶,吸滤泵,高锰酸钾,浓盐酸,3mol/L溴化钾溶液,3mol/L碘化钾溶液,淀粉溶液,装置如附图。 相似文献
3.
薛春荣 《常熟理工学院学报》2006,20(2):102-106,115
用同一种制备方法在玻璃和金衬底上分别制备有机高聚物薄膜;用原子力扫描显微镜对两种薄膜观测发现,高聚物—金属界面比高聚物—玻璃界面薄膜要平整、均匀的多,玻璃衬底上形成的高聚物界面高分子有明显的取向结构;用棱镜耦合法对两种不同衬底的高聚物薄膜波导进行同一条件下的m线观察,发现金属衬底上有机波导的m线要比玻璃衬底上有机波导的m线清晰。说明了衬底的不同会导致薄膜界面中的微观结构产生差异,这些差异会对波导的光学性能产生影响,解释了不同衬底的薄膜波导为何在光学性能上会出现差异。 相似文献
4.
专业实验目的是训练学生的专业技能,提高学生的综合素质.采用化学共沉淀法制备Ce0.8Sm0.2O1.9粉体,采用干压法压制成5×5×50 mm长条形样品和直径15 mm样片.用XRD对其结构进行表征,用阿基米德排水法和热膨胀仪对其致密度和烧结性能进行表征,用交流阻抗谱对其电学性能进行表征.通过实验,学生基本了解化学共沉淀方法的原理、致密度的测试方法以及电学性能的表征方法. 相似文献
5.
金属玻璃研究 总被引：1，自引：0，他引：1
姜左 《常熟理工学院学报》2000,14(4):53-55
讨论了金属玻璃的基本特性和结构特点,常用制备方法,介绍了金属玻璃的发展情况,并对金属玻璃的相分离及驰豫等进行了研究。 相似文献
6.
7.
《实验技术与管理》2017,(6)
将最新的科研成果引入实验教学,设计了纳米微晶玻璃的制备及性能表征综合实验。利用高温熔融冷却法制备玻璃基体,利用差热分析对其析晶性能进行分析;通过改变热处理温度及时间等工艺参数,对玻璃基体进行精密的热处理,获得一系列具有不同物化性能的微晶玻璃;最后利用X射线衍射仪、透射电镜、荧光光谱仪和分光光度计等现代分析测试手段对样品的性能进行表征与分析。结果表明,在620℃进行热处理2h后,可以从玻璃相中析出纯的NaYF4晶相,微晶颗粒尺寸约为27.3nm,通过Er3+/Yb3+稀土离子共掺可以获得最佳的光谱吸收和上转换发光性能。该实验涵盖知识点多且简单易行,有利于提高学生的综合运用知识和进行科研的能力。 相似文献
8.
采用Si元素替代形成玻璃合金Mg-Ni-Ln中的Ln系元素,形成Mg75Ni15Si10三元合金;通过震动浇注法向一模六腔的铜模型腔浇注,获得直径分别为￠3mm、￠4mm、￠5mm、￠6mm、￠7mm和￠8mm的6组圆柱试样,结果表明,￠3mm试样中有非晶态物质(块体金属玻璃)生成. 相似文献
9.
钢筋直径对粉煤灰混凝土粘结性能的影响 总被引：1，自引：0，他引：1
研究了钢筋直径对粉煤灰混凝土与钢筋粘结性能的影响.结果表明：钢筋与粉煤灰混凝土的粘结性能随着钢筋直径的减小而加强;同一外荷载作用下,钢筋直径为18mm的试件钢筋应变值比钢筋直径为22mm的试件大;钢筋直径为18mm的试件应力峰值的漂移更明显. 相似文献
10.
ITO薄膜的电学性能研究 总被引：2，自引：0，他引：2
以In金属和SnCl4·5H2 O作为原材料 ,采用溶胶一凝胶法在玻璃基体上制备了高质量的ITO薄膜 ,并分析了Sn掺杂时、热处理温度、热处理时间三种工艺参数对ITO薄膜电学性能的影响 ,确定了ITO薄膜的相组成 相似文献
11.
该文利用第一性原理计算对Mg60Cu30Y10合金进行了模拟研究,分析Mg60Cu30Y10合金的几何特征：双体关联函数、三体关联函数、空间关联系数,并利用Voronoi拼砌方法对Mg60Cu30Y10合金的结构做了分析.计算发现Mg60Cu30Y10合金中Mg原子的环境与晶态Mg2Cu中的环境类似,而Cu-Y、Y-Y之间的关联对于合金的性能起着决定性的作用. 相似文献
12.
In this paper, white light digital image analysis in frequency domination area for measuring 3D displacement is put forward. The measuring system has the characteristics of wholefield, non-contact and omnibearing measurement. It is simple and the coherent light is not demanded. Gray images before and after deformation are recorded using two CCDs at two different shooting angles, then digitalized and analyzed by frequency domination correlation arithmetic. The 2D displacement obtained is used to formulate 3D displacement via mathematical transformation, The experimental plate is 40 mm in length, 30 mm in width and 10 mm in height. The definite displacement is given using a 3D precise adjusting frame. The 3D displacement is calculated and compared with the definite displacement. The error is 4%-11% and the availability of this method was certified. Using this method, the compression deformation of a thin-wall cylinder with 140 mm in height, 64 mm in inner diameter and 64,6 mm in external diameter, was also measured. This method is proper to measure dynamic deformation. 相似文献
13.
Experiments were conducted using cohesionless sand particles with median diameter of 0.48 mm to investigate the time variation of sediment transport rate under the influence of local downward seepage.The experimental results show that the bedload transport rate in terms of volumetric sediment transport rate per unit width increased rapidly with time in the presence of suction,eventually reaching a peak beyond which it started to decrease.The trend of reduction was significantly reduced beyond 8 400 s after the test started.The analytical expression was derived in terms of dimensionless sediment transport rate and dimensionless time.The hypothesized relationships were compared with the experimental data,indicating a good agreement with each other. 相似文献
14.
The soil-water retention curve(SWRC)can be used to evaluate the ability of unsaturated soils to attract water at various water contents and suctions. In this study, drying SWRCs for a kind of sandy soil were obtained in the laboratory by using self-modified SWRC apparatus. In addition, the porosity and the pore size distribution of the samples were investigated by a mercury porosimetry test in order to analyze the effect of dry density. Results showed that the soil-water retention of the soil specimens was strongly dependent on the dry density. Under zero suction, soil specimens with a higher dry density exhibited lower initial volumetric water content. The higher the dry density of soil, the more slowly the volumetric water content decreased with the increase of suction. There was a general and consistent trend for a soil specimen to possess a larger air-entry value and residual suction, while smaller slope of SWRC when it had a higher density. This was probably attributed to the presence of smaller interconnected pores in the soil specimen with a higher dry density. The proportion of large diameter pores decreased in comparison to pores with small diameters in the soil tested. The measured total pore volume of the soil specimen, which had a larger dry density, was lower than that of the relatively loose specimens. 相似文献
15.
采用基于密度泛函理论的第一性原理平面波赝势方法研究了Au/SrTiO3(001)/Au异质结界面Y、Zr、Nb和Mo元素置换掺杂与电子传输相互作用的微观机制.通过分析各通道原子的电荷差分密度以及投影态密度,发现Au/SrTiO3(001)/Au中导电通道的开关状态对于不同界面掺杂金属元素差异明显.当Y和Zr分别置换界面层Ti(1)原子时,尽管界面电子态有局域化现象,但并没有改变理想界面模型导电通道的关闭状态;当Nb、Mo分别置换界面层Ti(1)原子时,电子掺杂效应使原来理想界面模型的导电通道从关闭状态转变为开放状态,从而提高了异质结界面体系的导电性能. 相似文献
16.
高玉杰 《淮南职业技术学院学报》2012,(3):11-15
通过对岩石乳化炸药、粉状乳化炸药、改性铵油炸药以及二级煤矿许用水胶炸药两种装药直径（Φ18mm和Φ35mm）进行爆速测试,研究炸药装药直径对爆速的影响,以及不同炸药装药直径变化对爆速增长率变化的影响。 相似文献
17.
作为一种新型材料,大块非晶合金的优良的力学、化学及物理性能使之在各行业中具有广泛的应用潜力．目前,对于块体非晶合金的制备工艺、脆性问题、塑性变形能力改善途径、韧化等方面的研究也越来越深入． 相似文献
18.
Bucket foundations[1 ,2]are a relatively newtype offoundation usedto support offshore structures .Each bucketfoundation consists of a thin cylindrical steel shell ,cappedwithalid of steel or concrete .Thefoundationcan penetrateinto sea floor when pumping … 相似文献
19.
利用较低纯度的原材料通过真空铜模吸铸法成功地制备了直径为2mm的（Fe0．5Co0．5）72B19．2Si4．8Nb4块体非晶合金。用X射线衍射（XRD）和示差扫描量热分析仪（DSC）研究了该非晶合金的晶化行为。结果表明,升温速率为10℃／min时,玻璃转变温度Tg为568．3℃,晶化起始温度Tx为598．6℃,晶化峰值温度Tp为608．0℃．随着升温速率的增加,特征温度Tg,Tx,Tp向高温区移动．用Kissinger法得到的玻璃转变激活能E。为272．3KJ／mo｜,晶化激活能E：为386．2KJ／too｜,晶化峰值激活能Ep为401．9KJ／mol,用Ozawa法得到的特征温度激活能与用Kissinger法得出的激活能变化趋势是一致的,都有Ep〉Ex〉Eg 此外,用Ozawa法分析了晶化激活能随晶化体积分数的关系,表明随着晶化体积分数的逐渐增加,激活能先增加,当晶化体积分数为14％时,激活能达到最大值379．4KJ／mol,然后随着晶化体积分数的逐渐增加,激活能减少。 相似文献
20.
The hot hardness behavior of Zr52.5Al10Ni10Cu15Be12.5 bulk metallic glass is studied from ambient temperature to the temperature over Tx （the onset crystallization temperature） using a hot macro-hardness tester and scanning electron microscopy （SEM）. The results show that the hot hardness behavior of Zr52.5Al10Ni10Cu15Be12.5 bulk metallic glass can be classified into 4 zones： the glassy zone in which the hardness almost linearly decreases with the increase of temperature, the viscoelastic zone in which the hardness is nearly unchanged, the viscous flow zone in which the hardness quickly tends towards near zero with temperature, and the crystallization zone in which the hardness sharply increases. The high temperature deformation behavior and the easy processable deformation region for bulk metallic glasses are also discussed on the basis of the hot marco-hardness. 相似文献