Ca对AE42镁合金的显微组织和拉伸性能的影响   总被引：1，自引：0，他引：1  

白晶  孙扬善  丁绍松  薛烽  汪黎 《东南大学学报》2004,20(1):43-48

AE42的铸态组织主要包含了α镁和少量的针状Al11RE3相, 呈典型的树枝晶分布. 少量Ca的加入使合金组织细化并形成新相Al2Ca, Al2Ca主要呈现分布在晶界的层片状形貌和弥散在晶粒内部的颗粒状形貌. 随着Ca的加入量增多, Al11RE3的体积百分比降低, 相应Al2Ca含量增加. 拉伸性能方面, Ca的加入使合金的屈服强度在室温和高温下都有显著提升, 随之延伸率有少量降低. Ca的加入还使合金在室温和150 ℃下抗拉强度下降. 温度的提高使Ca对抗拉强度的影响逐渐加大, 175 ℃和200 ℃下, 随Ca含量的增加抗拉强度逐渐增大.  相似文献   

Preparation and Characterization of M-Type Barium Ferrite Fibers via Aqueous Sol-Gel Process   总被引：1，自引：0，他引：1  

龚彩荣范国樑  宋崇林吕刚 《天津大学学报(英文版)》2007,13(2):117-120

BaFe12O19 fibers was prepared via an aqueous sol-gel process using Fe(OH)(HCOO)2 synthesized in laboratory and Ba(CH3COO)2 as the original materials and citrate as the chelate. The rheological behaviour of spinnable sol was characterized on rheometer, and the development of gel fibers to barium ferrite fibers was studied by IR, TG and XRD. Morphology observation of the fibers was given on SEM, and the diameter of the obtained fibers was between 5 and 10 μm corresponding to different additives. The additives affected the surface tension of the precursor sol which had close relation to the microstructure of fibers. Sucrose and hydroxyethylic cellulose could improve the surface tension while diethanolamine and hexadecylamine reduce that of the precursor sol. And using diethanolamine or hexadecylamine as an additive, well-structured BaFe12O19 fibers could be obtained.  相似文献   

变形速率对磨擦焊接头组织与性能的影响     

崔兰  霍立兴  张玉凤  荆洪阳  杨新歧  钱跃东 《天津大学学报(英文版)》2002,8(2):129-133

研究了变形速率对低合金结构钢 3 5CrMo磨擦焊接头组织与力学性能的影响 .结果表明 ,增加变形速率可改善焊缝韧性 .焊缝韧性改善的机理为近缝区晶粒细化和硬度降低 .采用金相法、TEM法对近缝区粒状组织精细结构进行了观察 ,粒状组织小岛由M -A组成 .指出增加变形速率使近缝区金属强化机制为位错强化、一定数量的岛状第二相强化和细晶粒强化 .通过测试异种金属焊缝界面近区碳浓度的分布 ,探讨变形速率对磨擦焊最高加热温度的影响 ,增加变形速率可使磨擦焊界面的最高加热温度下降  相似文献   

黄铜锭冶金质量对低压铸件组织与性能的影响     

洪丽华 《福建工程学院学报》2007,5(3):218-221

分析了黄铜锭的冶金质量对低压铸造水暖制件组织与力学性能的影响,结果表明铜锭冶金质量直接影响铸件的杂气含量与力学性能,对于不同冶金质量的铜锭(A、B),当成分相近时,经细化处理后铸件的结晶组织形态差别不大,夹杂相均为以PbO2为主、混有CuO2、ZnO或SiO2的氧化物复合夹杂,但铸件BC的夹气较多;在相同的熔体处理及成型工艺条件下,铸件AC的抗拉强度比Bc增加了16.3%,伸长率增加了26.6%.  相似文献   

Effects of parameters in femtosecond laser micromachining on ablation of silicon     

陈治  傅星  耿娜  胡小唐 《天津大学学报(英文版)》2009,15(3):225-228

A series of ablation experiments on silicon surface by femtosecond laser system of 775 nm and 150 fs duration pulses were carried out.The morphological characteristics and the associated effect in the ablation were tested by atomic force microscope (AFM),scanning electron microscope (SEM),focused ion beam (FIB),and the optic microscope.The single pulse threshold can be obtained directly.For the multiple pulses,the ablation threshold varies with the number of pulses applied to the surface due to the incubation effect.By analyzing the experimental data,the thresholds of laser fluences under various laser pulse numbers were obtained,and the relationships between ablation area and laser energy and laser pulse number were concluded.Meanwhile,the periodic ripple structure on silicon surface was found.Under the condition of certain laser power,the number of laser pulse can influence the formation of ripples.  相似文献   

红茂草营养器官的显微结构观察     

陈荃  邹亚丽  赵兰兰 《天水师范学院学报》2010,30(5):39-42

利用光学显微镜技术,采取石蜡切片法观察了红茂草营养器官的显微结构.结果表明：红茂草根的次生结构中有大量孔径不同的导管,但薄壁细胞数量较少;红茂草茎的维管束分散排列在基本组织中,皮层内有分泌腔分布,叶片上下表面均有大量表皮毛分布,叶肉组织中有1~2层的栅栏组织,中脉横切面上有三个靠得很近的维管束,可作为药材鉴别的参考.  相似文献   

甲基磺酸盐体系中的铜箔缎面镀锡     

王明杰  刘雪华 《福建工程学院学报》2009,7(1)

在以甲基磺酸锡为主盐、硫脲为电位调整剂的镀液体系中,在铜箔上制备了呈缎面光泽的均匀锡镀层.镀覆过程,用电偶电流法进行了分析;对所得镀层的显微组织结构,采用FE-SEM和XRD进行研究.结果表明,在该镀液体系中浸镀锡,镀覆过程迅速而平稳,所得锡镀层具有体心四方的晶体结构,镀层显微形貌为均匀分布的颗粒状形态.  相似文献   

高效熔体处理对易拉罐用铝材铸态组织和性能的影响   总被引：5，自引：0，他引：5  

陈永禄  傅高升  陈文哲 《福建工程学院学报》2003,1(4):11-15,54

用高效熔体处理技术制备试验用易拉罐用铝材，探讨了该技术对其铸态组织与力学性能的影响规律。结果表明：高效熔体处理可有效改善和提高易拉罐用铝材的冶金质量，与未处理相比，除杂率与针孔降低幅度分别为71．05％和94．49％，平均晶粒尺寸仅为76．5μm；晶界处第二相为(Al，Fe，Mn，Mg，Si，RE)或(A1，Fe，Mn，RE)复合相，呈短小骨骼状或小球状，晶内(A1，Mg)相呈细小颗粒状；拉伸断口为穿晶微孔聚集型断裂，与未处理相比，抗拉强度与伸长率分别提高16．6％及90．2％。  相似文献   

Structure characterization for the geopolymer of sodium silicate and metakaolin     

曹德光 《重庆大学学报(英文版)》2005,4(2):70-73

1 Introduction 1 During the last decade a new kind of material called geopolymer has emerged as a viable alternative for many conventional cements and plastics. Geopolymer is inorganic polymer derived from metakaolin and sodium silicate solution. It can be synthesized at low temperature and have useful properties such as high compressive strength. It is stable at temperatures up to 800 °C and even 1150 °C while ordinary Portland cement loses its strength at 500 °C [1]. Several microstruct…  相似文献   

钛合金表面激光熔覆氧化锆陶瓷涂层的显微组织     

李平  邓永瑞 《洛阳工业高等专科学校学报》1995,(3)

本文采用激光熔覆技术,探讨制备ZrO_2/Ti梯度功能材料,利用SEM和EPMA分析激光熔覆层,过渡层、热影响区的组织形貌和各组元的成份分布。用X射线衍射和微区X射线衍射技术分析激光熔覆区的氧化锆相变及各区域的相组成。得到:经过激光熔覆处理,熔覆区氧化锆由C—ZrO_2和T—ZrO_2组成,激光熔覆层、过渡区,热影响区的组织分别为ZrO_2枝晶 Ti_2O、粒状Z_rO_2 α相、片状α组成,在过渡区内成份是渐变的,组织为陶瓷相ZrO_2和塑性相α相混合。此工艺是制备ZrO_2/Ti梯度功能材料有前途的方法。  相似文献