金属焊接质量的红外成像检测     

王景中  徐小青 《上海海事大学学报》2001,22(3):214-216

介绍一种基于红外成像技术的金属焊接质量的无损检测方法.首先介绍了检测的基本原理和检测装置,然后详细给出了以边缘检测为基础的缺陷检测方法及检测结果.最后通过比较说明,利用红外成像技术对金属焊接质量进行无损检测是一种很有效的方法.  相似文献   

New insights into brazilwood lake pigments manufacture through the use of historically accurate reconstructions     

Tatiana Vitorino  Leslie Carlyle  Vanessa Otero 《文物保护研究》2016,61(5):255-273

A multi-analytical approach for the study of brazilwood and its lake pigments was carried out based on historically accurate reconstructions. Recipes for brazilwood lakes from the fifteenth century technical text Livro de como se fazem as cores and the Winsor & Newton nineteenth century colourman's archive were reproduced and compared. Both primary sources allowed for the successful preparation of brazilwood lake pigments with colours that vary from light pink to dark red. The main steps and ingredients for the manufacture of these pigments were common in both sources, particularly the addition of Al³⁺ in the form of alum, and calcium carbonate (chalk). Reconstructions revealed that the latter acts as a pH buffer and filler, controlling the pH at which the lake pigment precipitates. The main difference between the two sources is that the nineteenth century recipes give the quantities for all ingredients, the precise temperatures and time, and achieved higher relative pigment yields (75% versus 45%). Full chemical characterisation of the reconstructions provided detailed information on the individual steps in the pigment manufacture and revealed that the presence of calcium sulphate dihydrate (gypsum) in the final pigment was a result of its formation in situ. Infrared, reflectance, and fluorescence spectroscopy proved to be essential and complementary techniques: while infrared was used to characterise additives and binders, reflectance and fluorescence data were fundamental for identifying the chromophore. The pigments and paints produced can now be used as standards for the identification and investigation of brazilwood lake pigments found in artworks.  相似文献   

火焰原子吸收光谱法测定废水中不同价态铬的含量   总被引：1，自引：0，他引：1  

李淑新  许明远  马淑珍  曹继福 《唐山师范学院学报》2002,24(2):33-35

建立了火焰原子吸收光谱法测定不同价态铬含量的方法。该方法的检出限为0.029mg·L-1;相对标准偏差为0.54%;平均加标回收率为99.3%;利用此分析方法测定了废水中不同价态铬的含量,结果令人满意。  相似文献   

水杨酸铁的流变相合成和红外光谱   总被引：1，自引：0，他引：1  

冯致云李良超  苏克新 《荆门职业技术学院学报》2001,16(3):64-65

用流变相反应法合成了水杨酸铁配合物，对样品在4000—400cm^-1。范围内的主要红外光谱吸收峰进行了归属，通过元素分析、TG和IR确定该配合物的组成为Fe(HSal)3．3H2O(HSal=O-OHC6H4CO2)。  相似文献   

超支化聚酯的合成及在不同酸度下的聚集形态   总被引：5，自引：0，他引：5  

施彩娟  王康成 《湖州师范学院学报》2003,25(6):38-44

以苯-1，2，4-三羧酸-1，2-酐(BTAA)和二乙醇醚为原料合成超支化聚酯，在超支化聚酯的末端用4-氨基-1，8-萘酰亚胺(NVI)作荧光标记，得知在可见光区有强荧光的超支化荧光聚酯，酸度对NPI及荧光超支化聚合物有不同影响。  相似文献   

偶氮胂Ⅲ光度法测定微量稀土的实验教学改革     

林燕  鄢金  唐欢 《赣南师范学院学报》2011,32(3):97-99

对偶氮胂Ⅲ分光光度法测定稀土元素钆进行了条件优化实验,其中控制显色剂用量是提高测定准确度的关键.在显色溶液中加入无水乙醇以及采用双波长光度法可有效提高测定灵敏度.该实验项目已取代传统的光度分析实验,成为实验教学与实际应用相结合的典范.  相似文献   

Infrared Absorption Spectra of Serpentine Cat＇s Eye from Sichuan Province of China     

LU Bao - qi 《上海大学学报(英文版)》2005,9(4):365-368

Infrared （IR） absorption spectra and X-ray powder diffraction （XRD） patterrns of sexpenfine cat＇s eye from Sichuan Province have been investigated, and infrared absorption bands of the serpentine have been assigned in this paper. The results indicate that the bands near 3 600 - 3 700 cm^-1 belong to the stretching absorption band VOH, the bands in 948 - 1 100 cm^-1 axe assigned to the stretching vibraling band Usvo, and the bands at 600 570 and 440 cm^-1 respectively belong to the bending vibration band VOH, δMg-O and δSi-O. The serpentine cat＇ s eye includes two types： chrysotile and antigorite. Chrysotile has a sharp and intensive band at 3 688 cm^-1 and a weak band at 3 643 cm^-1 , while antigorite has only one intensive band in the region. At vibration band VSi-O, chrysotile and antigorite have a similar feature at 1 071 cm^-1, but the band at 980 cm^-1 in anfigorite has been split into two bands in chrysotile - a strong one at 1 027 cm^-1 and a weak one at 949 cm^-1. In addition, antigorite has a characteristic bending vibrating band δMg-O at 570 cm^-1. Based on the analysis of the feature of crystal structure, their IR differences axe well explained.  相似文献   

红外光谱法确认辽宁三地区苹果中黄烷醇类化合物     

侯冬岩  回瑞华  关崇新  王婧楠 《鞍山师范学院学报》2001,3(1):91-94

黄烷醇基本结构为C6·C3·C6型化合物 ,具有一定的抗癌活性 .其衍生形成的多酚类化合物对人体具有较强的抗衰老作用 ,它广泛存在于各种水果及一些植物中 .本文利用红外光谱法对辽宁三地区不同种类苹果的提取物进行了分析、比较 ,结果是辽南地区的苹果黄烷醇类化合物的含量少于辽西地区的苹果黄烷醇类化合物的含量 ,富士苹果的黄烷醇类化合物的含量高于国光苹果的黄烷醇类化合物的含量 ,为进一步研究开发提供了依据  相似文献   

智能车光电传感器和摄像头的选择     

戚玉婕 《扬州职业大学学报》2011,15(4):23-26

智能车设计综合了光学传感器、硬件电路和软件算法等多方面跨领域的知识技巧。本文针对黑白赛道智能车的赛道光学识别模块,系统地介绍了红外反射式光电传感器、激光传感器和可见光摄像头的实现原理及硬件电路;同时结合实际比较了其优缺点。  相似文献   

取代基酞菁铜的合成与表征     

夏道成  姚纪欢  韩双  马会宣  刘慧景 《雁北师范学院学报》2011,27(2)

首先以3,6-二羟基邻苯二甲腈和氯代正丁烷为起始反应物,在无水碳酸钾的催化作用下,经亲核取代反应,在DMF（N,N-二甲基甲酰胺）溶剂中合成了中间配体3,6-二丁氧基邻苯二腈,再以此配体和氯化亚铜为前体,采用DBU液相催化法合成了周边烷氧基取代的1,4,8,11,15,18,22,25-八丁氧基酞菁铜,经过元素分析、红外、荧光、紫外可见光谱和原子吸收表征证明,产物就是目标化合物取代基酞菁铜。  相似文献