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1.
《科技风》2017,(12)
本文对重庆某地区的白云石进行TG/DTG热分解实验,研究在氩气氛下白云石试样不同颗粒粒径的热分解,结果发现:白云石在氩气氛下的热分解受其粒径的影响。在氩气氛下,小粒径的白云石试样为一步分解,而大颗粒粒径的白云石表现出了异常的二步分解,这是由于在白云石内部的反应区附近产生一定的CO2分压。基于上述研究结果,对大颗粒粒径的白云石在氩气氛下进行进一步等温TG/DTG热分解实验,结果表明这种异常的二步热分解也与Ca CO3部分的低分解速率有关。  相似文献   

2.
采用机械球磨法制备了纳米Fe_2O_3样品。利用扫描电子显微镜(SEM)、X射线衍射仪(XRD)、能谱仪(EDS)、透射电子显微镜(TEM)表征了Fe_2O_3粉末的晶体结构和微观形貌。同时,研究了纳米Fe_2O_3对高氯酸铵(AP)的催化作用。结果表明,纳米Fe_2O_3粒径约为100nm,类呈球形,球磨过程无杂质引入。DSC分析表明,一定掺杂量(1%,3%,5%,)的纳米Fe_2O_3对AP具有显著的催化作用,且随着掺杂量的增高,AP热分解的低温反应峰逐渐消失,高温反应峰增强,峰温降低(ΔT在40℃~61℃)。  相似文献   

3.
合理的氩气纯度可以提高焊接质量。本文研究在同等条件下,纯度为99.99%、99.995%、99.999%的氩气对焊接质量的影响程度,对在给定工艺参数下,用3 mm,厚6082铝合金薄板进行脉冲MG焊接试验,焊接试验完成后,分别用X-Ray检测仪、游标卡尺、精密焊缝尺、万能试验机对成形后的焊缝进行表征。结果表明:在相同条件下,在纯度为99.99%、99.995%、99.999%氩气保护下的焊出的焊缝外观和焊缝内部气孔生成情况无明显差异,且99.99%氩气焊缝熔宽和余高最小;纯度为99.99%、 99.995%、99.999%的氩气保护下的焊缝抗拉强度约为21 9MPa、1 92.5MPa和21 7MPa,约为母材抗拉强度的67%、59%和66%;三种氩气纯度均能满足焊接质量要求。  相似文献   

4.
研究了电解二氧化锰(EMD)粉体在不同缝制方法吨袋中吸附水含量的变化,结果表明:吨袋储存的EMD粉体吸附水含量增加较多,储存3.5个月其110℃烘箱水分为1.76%,储存4.5个月110℃烘箱水分达1.90%,则已超过产品规格上限,其他改进吨袋防水效果较好。即使使用普通吨袋,仓库存放3.5个月和4.5个月经筛分EMD也不会结块。  相似文献   

5.
采用热重法(TG)和微分热重法(DTG)研究了2-(4-羧基苯基)-5-氨基-6-羟基苯并噁唑(CAB)在氮气氛或氧气氛中的热分解过程,CAB在氮气氛中的热分解过程是一个四阶段过程。运用量子化学从头计算法软件GAMESS计算了CAB分子的键级,测定了CAB及其在热分解过程中不同阶段产物的红外光谱,并由此得出CAB在氮气氛中的热分解机理;根据CAB在不同升温速率下的热重曲线数据计算出其特征热分解反应动力学表观失重活化能(E)和指前因子(A)。  相似文献   

6.
空气气氛中滑石的热分解动力学实验研究   总被引:1,自引:0,他引:1  
含水矿物的热分解动力学研究对于了解俯冲带中-深源地震的成因机制具有重要意义.本文用综合热分析仪(TG-DSC)研究滑石在动态空气气氛下的热分解过程,利用热重(TG)数据对滑石的热分解动力学进行分析.利用Friedman法和FWO法,分别计算滑石热分解过程中的表观活化能Ea和指前因子A,并以Friedman法求得的活化能为初始值,通过非线性回归拟合得到热分解过程最可能的反应机理和动力学参数.研究结果表明,滑石在830~1 050℃内发生热分解,此过程为n级反应,表观活化能Ea为344.2 k J/mol,指前因子A为4.9E12 s-1.  相似文献   

7.
硫酸亚铁铵常以水合物形式存在,其水合物为浅蓝绿色单斜晶体,俗称摩尔盐,是一种复盐。在空气中一般比较稳定,不易被氧化,溶于水而又不溶于乙醇,受热到100℃时失去结晶水。  相似文献   

8.
采用生物发酵法从葡萄糖直接制备葡萄糖酸锰,实验表明温度31℃、摇床转速200 r/min、碳酸锰的添加时刻12 h,其发酵转化率为93.01%,产品的结构经元素分析和IR确证.  相似文献   

9.
黄普乐  孙崇波  谢鸣 《科技通报》2009,25(4):423-426,431
研究结果表明:高温和GA3处理均能有效解除彩色马蹄莲种球休眠,促进其发芽,而其中高温的作用更加明显."高温(22℃~25℃)+GA3(300 mg/kg,15 min)"处理对促进彩色马蹄莲种球发芽,解除休眠的效果最好,在60 d和80 d后发芽率分别达到53.3%和93.3%;并初步明确了球淀粉含量的降幅和种球的发芽率成正相关.一年生种球的最佳促进开花处理为"高温(22℃~25℃)+GA3(200 mg/kg,10 min)",处理后开花率约为36.7%.二年生种球、三年生种球的最佳处理为"高温(22℃~25℃)+GA3(300 mg/kg,10min)",处理后开花率分别为66.7%和83.3%.  相似文献   

10.
本实验分别以硝酸铜和硫化钠作为铜源和硫源,溶解在乙二醇(EG)中,在十二烷基苯磺酸钠(SDBS)的作用下,通过溶剂热法成功制备了球状纳米级硫化铜光催化剂。通过扫描电子显微镜(SEM)和X射线衍射(XRD)对产物进行表征,结果证实产物为高纯度的球状纳米级硫化铜。最后在长弧汞灯照射下,对其光催化降解性质进行了研究。紫外可见吸收光谱表明:棒状纳米级Cu S具有很高的光催化活性,在模拟日光照射下对甲基橙(MO)和亚甲基蓝(MB)的降解率分别达到94.8%和91.6%。  相似文献   

11.
This study examined how students who had no prior experience with videoconferencing would react to the use of videoconferencing as an instructional medium. Students enrolled in seven different courses completed a questionnaire at the beginning of the semester and again at the end of the semester. Students at the origination and remote sites did not differ in their reactions toward videoconferencing but there was a significant difference for gender. Women reacted less favorably to videoconferencing. Compared to the beginning of the semester, students reported significantly less positive attitudes toward taking a course through videoconferencing at the end of the semester. There were no significant differences in students' attitudes toward videoconferencing across courses at the beginning of the semester but there were significant differences across the courses at the end of the semester. The results suggest the need for better preparation for both students and instructors.  相似文献   

12.
Ajoint study by Prof. ZHANG Zhibin from the CAS Institute of Zoology and his co-workers from Norway, US and Swiss have indicated that historical outbreaks of migratory locusts in China were associated with cold spells, suggesting that China's projected climate warming could decrease the pest's numbers. The study was published in Proceedings of theNational Academy of Sciences on 17 September, 2007.  相似文献   

13.
A computer-mediated group is a complex entity whose members exchange many types of information via multiple means of communication in pursuit of goals specific to their environment. Over time, they coordinate technical features of media with locally enacted use to achieve a viable working arrangement. To explore this complex interaction, a case study is presented of the social networks of interactions and media use among members of a class of computer-supported distance learners. Results show how group structures associated with project teams dominated who communicated with whom, about what, and via which media over the term, and how media came to occupy their own communication niches: Webboard for diffuse class-wide communication; Internet Relay Chat more to named others but still for general communication across the class; and e-mail primarily for intrateam communication. Face-to-face interaction, occurring only during a short on-campus session, appears to have had a catalytic effect on social and emotional exchanges. Results suggest the need to structure exchanges to balance class-wide sharing of ideas with subgroup interactions that facilitate project completion, and to provide media that support these two modes of interaction.  相似文献   

14.
CAS should stick to the principle of rendering service to, and giving impetus for, the development of China's science enterprise by making S&T innovations, said CAS President LU Yongxiang. The CAS president made the remarks in a recent talk to communicate the gist of the winter session of the Party's Leading-member Group at CAS, which was held from 7 to 11 January in Beijing.  相似文献   

15.
With great care, Dr. ZHOU Zhonghe takes out a package wrapped by cotton tissue from a drawer and says: "This is the gem of our collections: the fossil of a bird that lived 125 million years ago!" Then, pointing at a tiny mound, he explains: "Look, this is the claw and that is the head. It was in the egg shell and ready to hatch ... The species fell into a family of waterside inhabitants."  相似文献   

16.
Electronic data interchange (EDI) provides means for interorganizational communication, creates network externalities, requires an advanced information technology (IT) infrastructure, and relies on standards. In the diffusion of such innovations, institutional involvement is imperative. Such institutions contain governmental agencies, national and global standardization organizations, local government, and nonprofit private organizations like industry associations. The last type of organizations we call intermediating institutions. They intermediate or coordinate ("inscribe") the activities of a group of would-be adopters. Unfortunately, little is known of how these organizations shape the EDI diffusion trajectory. In this article we examine one specific type of intermediating organizations?industry associations?and how they advanced the EDI diffusion process in the grocery sectors of Hong Kong, Denmark and Finland. We identify six institutional measures, placed into a matrix formed by the mode of involvement (influence vs. regulation) and the type of diffusion force (supply push vs. demand pull), that can be mobilized to further the EDI diffusion. Industry associations were found to be active users of all these measures to varying degrees. Their role was critical especially in knowledge building, knowledge deployment, and standard setting. Furthermore, institutional involvement varied due to policy and cultural contingencies and power dependencies.  相似文献   

17.
The increasing prospects of digital piracy has prompted the perceived need by electronic publishers to adopt technical systems of protection, and governments to reform their copyright laws. This article is a preliminary study of the management of intellectual property by electronic publishers, defined as those involved in the production of online databases, and CD-ROMs. It focuses on three main issues: (1) how electronic publishers view the increasing threat of piracy; (2) the methods of protection employed to protect intellectual property in digital format; and (3) the importance of technological protection of intellectual property in electronic publications. The analysis is based on a sample of 23 UK electronic publishers. The interviews revealed an interesting assortment of protection methods and did not show that technological protection was a preferred way. Instead, the means of protection, in addition to copyright law, comprised niche markets, pricing, trust, bad publicity, and nontechnical and technical means.  相似文献   

18.
Long-standing conflict between domain name registrants and trademark holders prompted the Internet Corporation for Assigned Names and Numbers (ICANN) to create a global, mandatory arbitration procedure known as the Uniform Dispute Resolution Policy (UDRP). The UDRP has been used in 2166 cases involving 3938 domain names as of 1 November 2000. The policy gives the initiator of a complaint, generally a trademark holder, the right to choose which ICANN-accredited dispute resolution service provider (RSP) will handle the case. During the preparation of the UDRP,some feared that complainant selection would lead to "forum shopping" that might bias the results. This article performs a statistical assessment of the forum-shopping thesis and finds support for it. There are statistically significant differences in the various RSPs' propensity to take away names from defendants; there are also major differences in the number of cases brought to each RSP. RSPs who take away names have the larger share of cases. The study examines other variables that might explain differences in market share, such as price, the plaintiff's nationality, or the time taken to decide a case. It finds that nationality and time also are correlated with market share. The study concludes that shopping for a favorable outcome is an important factor in the UDRP.  相似文献   

19.
Prof. Raymond C.K. Chen, a neuropsychologist with the CAS Institute of Psychology, has made novel progress in his studies of schizophrenia. His work has been reported by a recent issue of Behavioural Neurology.  相似文献   

20.
The main premise of this article is that in information societies generally, and in virtual social contexts particularly, a distinctive style of interaction to facilitate the communication of difference, heterotopic communication , has emerged. It rests on two cultural foundations: an ideological belief in the positive, socially integrating power of communication, and a prevailing ethic of instrumental rationality, subjective individualism, and strategically practiced self-interest. The former is demonstrated by the use of simulation and spectacle as sources of information; exhibitionism/voyeurism as a communicative style; and the awareness of surveillance. The latter is seen in the competitive use of knowledge as a commodity; a surface globalism masking deep parochialism; lateral as well as vertical information inequity; and the use of public versus private as strategies for engagement rather than as spaces. Those who engage in heterotopic communication resort to their 'own devices' both in the sense of personal agendas, strategies, interests, and interpretations, and in the form of the telecommunication tools that help realize them. These personal and technological devices allow individuals with the right educational and technical resources to avoid exposure to disagreement, difference, or other information that does not serve their direct purposes or reflect their particular views of the world; yet they also help convey the appearance of openness, availability, and cooperation. This style of interaction is used strategically in combination with information and communication technologies to gain social or economic advantages, but it may encourage social separatism and parochialism, inhibit the negotiation of disputes, and emphasize competing interests.  相似文献   

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