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101.
采用液态镓作为离子源的FIB系统在材料科学研究领域可以起非常重要的作用。离子束聚焦于样品表面,在不同大小、束流及通入不同辅助气体的情况下,可分别实现图形刻蚀、绝缘和金属膜的沉淀,扫描离子成像等功能。该系统有三大用途:形貌观察,分辨率高达5nm;微刻蚀以及微沉淀。本文介绍了FIB技术的应用。  相似文献   
102.

Objective

This study explored the effects of different light curing modes and ethanol-wet bonding on dentin bonding strength and durability.

Methods

A total of 54 molars were randomly divided into three groups: Single Bond 2, Gluma Comfort Bond, and N-Bond. Based on the three light-curing modes and presence or absence of ethanol pretreatment, the samples were assigned to six subgroups: high-light mode, ethanol pretreatment+high-light mode, soft-start mode, ethanol pretreatment+soft-start mode, standard mode, and ethanol pretreatment+standard mode. All samples were bonded with resin based on the experimental groups. After 24 h and 6 months of water storage, a universal testing machine was used to measure microtensile bond strength. Scanning electron microscopy (SEM) was applied to observe mixed layer morphology.

Results

The 24-h and 6-month microtensile bond strengths of the ethanol pretreatment groups were significantly higher than those of the non-ethanol pretreatment groups at the same light modes (P<0.05). With or without ethanol pretreatment, the microtensile bond strengths of the high-light modes were significantly lower than those of the soft-start modes and standard modes (P<0.05). The microtensile bond strengths of samples from the 6-month water storage group significantly decreased compared with those of samples from the 24-h water storage group (P<0.05). The soft-start groups and standard groups formed better mixed layers than the high-light mode groups, whereas the ethanol pretreatment groups formed more uniform mixed layers than those without ethanol pretreatment.

Conclusions

Ethanol-wet bonding technique, soft-start, and standard modes could improve dentin bonding properties.
  相似文献   
103.
The concept and existence of learning styles has been fraught with controversy, and recent studies have thrown their existence into doubt. Yet, many students still hold to the conventional wisdom that learning styles are legitimate, and may adapt their outside of class study strategies to match these learning styles. Thus, this study aims to assess if undergraduate anatomy students are more likely to utilize study strategies that align with their hypothetical learning styles (using the VARK analysis from Fleming and Mills, 1992 , Improve Acad. 11:137–155) and, if so, does this alignment correlate with their outcome in an anatomy course. Relatedly, this study examines whether students’ VARK learning styles are correlated with course outcomes regardless of the students’ study strategies, and whether any study strategies are correlated with course outcomes, regardless of student-specific VARK results. A total of 426 anatomy students from the 2015 and 2016 Fall semesters completed a study strategies survey and an online VARK questionnaire. Results demonstrated that most students did not report study strategies that correlated with their VARK assessment, and that student performance in anatomy was not correlated with their score in any VARK categories. Rather, some specific study strategies (irrespective of VARK results), such as use of the virtual microscope, were found to be positively correlated with final class grade. However, the alignment of these study strategies with VARK results had no correlation with anatomy course outcomes. Thus, this research provides further evidence that the conventional wisdom about learning styles should be rejected by educators and students alike. Anat Sci Educ. © 2018 American Association of Anatomists.  相似文献   
104.
105.
We report differential phase contrast scanning transmission electron microscopy (TEM) of nanoscale magnetic objects in Kagome ferromagnet Fe3Sn2 nanostructures. This technique can directly detect the deflection angle of a focused electron beam, thus allowing clear identification of the real magnetic structures of two magnetic objects including three-ring and complex arch-shaped vortices in Fe3Sn2 by Lorentz-TEM imaging. Numerical calculations based on real material-specific parameters well reproduced the experimental results, showing that the magnetic objects can be attributed to integral magnetizations of two types of complex three-dimensional (3D) magnetic bubbles with depth-modulated spin twisting. Magnetic configurations obtained using the high-resolution TEM are generally considered as two-dimensional (2D) magnetic objects previously. Our results imply the importance of the integral magnetizations of underestimated 3D magnetic structures in 2D TEM magnetic characterizations.  相似文献   
106.
利用长链烷烃取代基与石墨表面的较强相互作用,可以获得烷基取代的有机小分子(酞菁、卟啉、碱基)的高分辨STM图像.理论分析表明,这些分子的吸附稳定性来源于长链烷基与石墨间较强的范德华相互作用,以及长链烷烃链间的二维结晶能.分子在表面的吸附组装结构受到分子与基底间、吸附分子间,以及溶剂与分子间作用的共同影响.对于长链烷基取代的碱基分子在石墨表面的组装结构中,分子的排列方式不仅受到烷基链与石墨间较强的取向匹配的作用,碱基分子间形成的多个氢键以及芳环离域π键的作用也会影响分子的排列方式,并且是造成烷基取代碱基分子组装结构多样性的原因.扫描隧道谱研究表明,硫醇在Au表面的自组装分子膜对电流的整流作用,来自于分子中巯基与Au表面形成的双电层,而不对称取代的NtBuPc分子在石墨表面的LB膜的电流整流行为,来源于分子内部的不对称电子结构.  相似文献   
107.
力竭运动大鼠心肌心钠素表达的变化   总被引:40,自引:4,他引:36  
为了探讨力竭运动对大鼠心脏心钠素表达的影响,采用4月龄雄性XD大鼠,体重220g-360g,随机分为(1)正常对照组(A组),(2)有训练游泳力竭组(B组)、(3)无训练游力竭组(C组),每组各14只。灌注后取出整心,用免疫组化ABC法,结果是:心钠素免疫阳性反应为:右心耳〉右心房〉左心房〉右心室近心房处,与A组相比,B组大鼠心房肌心钠素阳性择应明显增强,心钠素电子致密颗粒大量增加;C组大鼠心房钠  相似文献   
108.
我们用兔抗人α-actinin(α-辅肌动蛋白)抗血清和羊抗兔IgG-胶体金复合物作为标记物,在由Lowicryl K4M包埋的组织超薄切片上定位Z带蛋白α-actinin。在大负荷斜蹲后48小时从6名男性受试者(年龄为22—22岁)的两侧腿股外肌中取得活检样品,并在运动后不同时刻及活检取样前对随机确定的每一受试者的一条腿进行针刺或静力牵张,另一侧腿作对照。结果发现,针刺或静力牵张腿Z带特异性标记密度比其对照腿高。此外,针刺或静力牵张还能使Z带发生超微结果的变化率分别减少36%和22%,并使显著变化的比例减少,轻度变化的比例增加。以上观察结果揭示了针刺或静力牵张能抑制由于α-actinin的解聚或降解引起的Z带超微结构变化过程,或者通过加速α-actinin的聚合或合成而促进Z带超微结构的恢复。  相似文献   
109.
Defects exist ubiquitously in crystal materials, and usually exhibit a very different nature from the bulk matrix. Hence, their presence can have significant impacts on the properties of devices. Although it is well accepted that the properties of defects are determined by their unique atomic environments, the precise knowledge of such relationships is far from clear for most oxides because of the complexity of defects and difficulties in characterization. Here, we fabricate a 36.8° SrRuO3 grain boundary of which the transport measurements show a spin-valve magnetoresistance. We identify its atomic arrangement, including oxygen, using scanning transmission electron microscopy and spectroscopy. Based on the as-obtained atomic structure, the density functional theory calculations suggest that the spin-valve magnetoresistance occurs because of dramatically reduced magnetic moments at the boundary. The ability to manipulate magnetic properties at the nanometer scale via defect control allows new strategies to design magnetic/electronic devices with low-dimensional magnetic order.  相似文献   
110.
Anti-seismic behavior of HRB400 reinforced steel bars   总被引:1,自引:0,他引:1  
1 Introduction Steel bar is one of the most important constructional materials ensuring the safety of buildings, and sufficient anti-seismic strength is required when it is applied to buildings in the region where an earthquake might occur. HRB335 steel bars are being used in China while 400 MPa steel bars are wildly used in Europe [1]. To ensure the security of buildings, 400 MPa steel bars have been developed in China. Before these steel bars being wildly used, a full-scale survey of the…  相似文献   
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