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Comparison of oil and egg tempera paint systems using time-of-flight secondary ion mass spectrometry
Zachary E. Voras Kristin deGhetaldi Brian Baade Eric Gordon Glenn Gates Thomas P. Beebe 《文物保护研究》2016,61(4):222-235
Time-of-flight secondary ion mass spectrometry (ToF-SIMS) is quickly becoming a critical tool in the field of art conservation. This technique provides high-resolution spatial maps of both inorganic and organic components located within cross-sectional samples collected from works of art. With recent advances in surface analysis, ToF-SIMS can now be used to identify specific amino acids present in protein-containing materials as well as fatty acids in drying oils. For example, the detection of the ion fragment associated with the amino acid hydroxyproline can be used to confirm the use of animal glue in a paint sample. As an analytical technique, ToF-SIMS avoids the need for derivatization/silylation reagents, with no interference by the presence of pigments. Furthermore, the layered systems that are often encountered in historical paint samples remain intact throughout the analytical procedure. This allows for the co-localization of organic and inorganic species in specific layers (e.g. egg yolk paint atop a glue ground). Because of this ability to localize the analytical signal to approximately 6?µm or less, the mass spectral information can be used to produce mass-resolved and spatially-resolve images which can be correlated to previous studies of the same samples. In this study, ToF-SIMS was used to analyze a paint cross section obtained from a painting attributed to Raphael, and another from a painting by the Sienese artist Matteo di Giovanni. 相似文献
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Beatrice S. Bartlett 《Archival Science》2007,7(4):369-390
This article describes the first half century of the Communist government’s supervision and management of the central-government
archives of the last two dynasties. Immediately with the Communist ascent to power in 1949, the new government took great
interest in assembling and protecting the country’s archival documents, readying the Ming-Qing archives for access to scholars,
and preparing for publication of selected materials. By the 1980s Beijing’s Number One Historical Archives, in charge of the
largest holding of Ming-Qing documents, had become the first Chinese authority to complete a full sorting and preliminary
catalogues for such a collection. Moreover, to facilitate searches, an attempt has recently begun to create a subject-heading
system for these and other holdings in the country. In the first half century’s final decades, foreign researchers were admitted
for the first time and tours and international exchanges began to take place.
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Beatrice S. BartlettEmail: |
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Rena Beatrice Goldstein 《Educational theory》2019,69(5):646-652
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Beatrice Avalos 《Teaching and Teacher Education》2011,27(1):10-20
A review of publications in Teaching and Teacher Education over ten years (2000-2010) on teacher professional development is the subject of the paper. The first part synthesises production referred to learning, facilitation and collaboration, factors influencing professional development, effectiveness of professional development and issues around the themes. The second part, selects from the production nine articles for closer examination. The paper concludes by noting how the production brings out the complexities of teacher professional learning and how research and development have taken cognisance of these factors and provided food for optimism about their effects, although not yet about their sustainability in time. 相似文献
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