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1.
采用电弧离子镀工艺,调节N2分压制备了系列(Ti,A1)N硬质涂层,研究了不同N2分压对涂层表面形貌、相结构、成分及力争性能的影响.结果表明,当氮气分压较低时,涂层金属相含量较高,涂层硬度和残余应力较低,膜/基结合力较高,涂层耐磨性较差;当氮气分压较高时,涂层氮化物相含量较高,涂层硬度和残余应力较高,膜/基结合力偏低,涂层耐磨性很强.  相似文献   

2.
The objective of the present research is to investigate the relationship among tool wear, surface topography, and surface roughness when high-speed end milling Ti-6Al-4V alloy, and also to define an optimal flank wear criterion for the cutting tool to integrate tool life and the surface roughness requirements of the finish milling process. An annealed Ti-6Al-4V alloy was selected as the workpiece material, undergoing end milling with uncoated carbide inserts. The flank wear of the insert was observed and measured with the toolmaker's microscope. To examine machined surfaces, 3D surface topography was provided by the white light interferometer, and the arithmetical mean roughness (Ra) was calculated with the WYKO Vision32 software. The flank wear increases with cutting time, and the maximal flank wear is set as the flank wear criterion. As the cutting process progresses, tool wear is the predominant factor affecting the variation of surface roughness. According to the plots for the tool wear propagation and surface roughness variation, an optimal flank wear criterion can be defined which integrates the tool life and the surface roughness requirements for the finish milling process.  相似文献   

3.
结合溶胶-凝胶法和化学镀方法,于镁合金基材表面成功制备了均匀的复合Ni-P-SiO_2/TiO_2/Al_2O_3镀层,采用扫描电镜(SEM)、光学显微镜(OM)、摩擦磨损试验及电化学方法,对比研究了Mg基材、基础Ni-P镀层与3种复合镀层的显微组织结构、耐磨性及耐腐蚀性。结果表明,加入3种溶胶所制备的复合镀层较Mg基材大幅度提高耐磨性和耐腐蚀性;3种复合镀层较Ni-P镀层具有更加均匀、致密的显微形貌,减少了直接加入纳米粉末的团聚,同时耐磨和耐蚀性改善。其中Ni-P-SiO_2复合镀层具有较高的显微硬度(HV513)和最低的摩擦系数(0.34),最高的腐蚀电位(-1.18V)及较小的腐蚀电流密度(9.5×10~(-3)mA·cm~(-2))。综合制备最佳工艺,并考虑节能减排因素,Ni-P-SiO_2复合镀层可作为性能优良的Mg合金耐磨、耐腐蚀镀层使用,于实际工业生产大有裨益。  相似文献   

4.
To improve the oxidation resistance and corrosion resistance of Zr-4 alloy, titanium nitride(TiN) coatings were prepared on the Zr-4 alloy with a TiN ceramic target with different ratios of N_2. Microstructure and high-temperature properties of the TiN coated samples were studied by scanning electron microscopy(SEM), energy dispersive spectrometer(EDS), X-ray diffraction meter(XRD), X-ray photoelectron spectroscopy(XPS), heat treatment furnace and autoclaves, respectively. The x value of the TiN coatings(TiN_x) ranges from 0.96 to 1.33. After the introduction of N_2, TiN coating exhibits a weak(200) plane and a preferred(111) orientation. The coating prepared with an N_2 flow ratio of 15% shows an optimal oxidation resistance in the atmospheric environment at 800 °C. In either 1 200 °C steam environment for one hour, or deionized water at 360 °C and a pressure of 18.6 Mpa for 16 d, the opitimized TiN coated samples have no delamination or spallation; and the gains in the masses of samples are much smaller than Zr-4 alloy. These results demonstrate the effectiveness of the optimized TiN coating as the protective coating on the Zr-4 alloy under extreme conditons.  相似文献   

5.
研究了一种新的、简便的、环保的铝及铝合金化学镀镍新工艺,探讨了前处理、光亮剂添加量对镀层质量的影响。结果表明,铝及铝合金经过自制浸锌剂二次浸锌后,每升镀液中添加15mL光亮剂所获得的样品镀层均匀、结合力最佳。  相似文献   

6.
Aiming at the surface integrity of titanium alloy Ti-6Al-4V in high speed side milling, a series of side mill- ing tests were carried out with uncoated carbide milling cutter at various milling speeds. Surface roughness, residual stress, subsurface microstructure and microhardness variations were investigated. The surface roughness measurement results present that the milling speed from 80 to 120 m/min fails to produce better and more stable roughness values compared with the result obtained from 320 to 380 m/min. The residual stresses in the feed direction and axial depth of cut direction are in similar trends for the two milling speed levels mentioned above. Moreover, the residual stress pro- duced at 320 to 380 m/min is lower and more stable than that at 80 to 120 m/min. The microstructure analysis shows that the volume of β phase in the near surface becomes smaller and the deformation of β phase in the near surface be- comes obvious with the increase of the milling speed. Subsurface microhardness variation was observed down to 200 μm below the machined surface at 80 to 120 m/min and down to 160 μm at 320 to 380 m/min. It is concluded that better surface integrity and higher material removal rate can be obtained at 320 to 380 m/min than at 80 to 120 m/min.  相似文献   

7.
INTRODUCTION Monocrystalline SBN (Strontium barium nio-bium, SrxBa1?xNb2O6, denoted SBNx?100, where 0.25≤x≤0.75) solid solution, is currently being inves-tigated as potential material for many micro-device applications, such as piezoelectric infrared detectors, piezoelectric, electro-optic modulators, and holo-graphic storage (Koch et al., 1998), because SBN has one of the largest known linear electro-optic coeffi-cients (r33=1300 pm/V for SBN75), two orders of magnitude larger th…  相似文献   

8.
为改善低温镀铁工艺镀层的耐磨损耐腐蚀性能,提高镀层表面硬度,以GKDM系列高频脉冲电镀电源为实验复合电沉积工艺电源并配合超声.机械搅拌制备纳米Fe-ZrO2镀层。研究了高频脉冲电源参数:峰值电流导通(TON)、关闭(TOFF)时间;一组正脉冲(TF)负脉冲(TR)的工作时间对镀层表面纳米含量的影响。结果表明当GKDM系列高频脉冲电源TON=20×0.1ms,TOFF=80×0.1ms时,纳米沉积分布均匀致密,质量分数高。  相似文献   

9.
概述了铝合金几种先进的焊接方法:钨极氩弧焊、电子束焊、激光焊及搅拌摩擦焊。重点介绍了铝合金最有前途的固相连接方法——搅拌摩擦焊,并展望了铝合金搅拌摩擦焊的应用前景。指出搅拌摩擦焊是铝合金最好的连接工艺,应深入研究。  相似文献   

10.
对铝基体上形成的Ni-P合金镀层的组织结构进行了探讨,结果表明:非晶态Ni-P合金镀层以层片状沉积,表面具有胞状结构,镀层的磷含量及热处理温度对Ni-P合金层的组织结构有影响。  相似文献   

11.
选择含氮节镍型QN2109Mo奥氏体不锈钢作为研究对象,采用XRD、TEM、SEM、EDS、摩擦磨损试验机和电化学工作站等检测手段,研究QN2109Mo不锈钢的组织结构、摩擦磨损性能以及耐腐蚀性能,并与316L不锈钢进行对比。实验结果表明:N原子主要以间隙固溶形式存在于QN2109Mo不锈钢中,对QN2109Mo不锈钢组织起到了细化作用,提高了QN2109Mo 不锈钢的硬度。在干摩擦状态下,QN2109Mo不锈钢的耐磨损性能优于316L不锈钢,其磨损机理为氧化磨损和磨粒磨损共同作用。在w(NaCl)为3.5%的溶液中,QN2109Mo不锈钢表现出比316L不锈钢更低的自腐蚀电流密度和更高的点蚀电位,具有更优异的耐NaCl 溶液腐蚀性能。  相似文献   

12.
采用磁控溅射方法在Si片沉积了Ti-50.9at%Ni形状记忆合金薄膜,并将薄膜分别在不同温度下进行退火.利用示差扫描量热方法(DSC)、X射线衍射仪(XRD)、透射电镜(TEM)研究了薄膜退火前后形貌、相变特征及应力随退火温度的变化.实验结果表明:溅射态薄膜为非晶态,其晶化温度范围为430℃-535℃,晶化同时伴随着Ti3Ni4相的析出;退火后的薄膜随着退火温度的升高,Rs、Af、Ms均呈上升趋势.薄膜的残余应力随着退火温度的增加而逐渐减少.  相似文献   

13.
前混合水射流喷丸强化表面粗糙度预测   总被引:1,自引:0,他引:1  
选择对喷丸表面粗糙度起主要影响作用的喷丸压力、喷嘴扫描速度和靶距3个因素,各6个水平,选用直径为0.25 mm的玻璃弹丸,应用前混合水射流对2A11铝合金进行喷丸试验;采用针描法和SJ-201 Surface Roughness Tester测量喷丸表面粗糙度;基于表面粗糙度试验数据,应用多元线性回归和多项式回归分析方法建立喷丸表面粗糙度数学模型,并将模型应用于喷丸表面粗糙度预测,研究表明:多元线性回归预测模型,计算精度高、泛化能力强、预测效果好,平均相对误差为13.37%,能够满足工业生产对喷丸表面粗糙度预测精度的要求,具有较大的实用价值.  相似文献   

14.
针对当前国内外无铅化趋势的要求,简单比较了多种锡系合金可焊镀层的优缺点,提出纯锡可焊镀层的研究方向,并开发出一种纯锡电镀的添加剂,最后从外观、可耐焊、润湿效果、加速氧化、端头拉力等方面,对Sn-Pb镀层和纯锡镀层进行了比较,发现纯锡镀层的各种性能均不弱于Sn-Pb镀层,部分性能还要优于Sn-Pb镀层.另外,本文对各种焊膏的性能也作了比较.  相似文献   

15.
316不锈钢海水泵叶轮,使用10~12月后损坏严重。对叶轮失效原因分析表明:叶片减薄严重的主要原因是高流速海水中的固体颗粒(粉砂)的磨削作用加速的磨损腐蚀。选择对316不锈钢叶轮采用表面高分子涂耐磨涂层的方案可延长叶轮使用寿命,且更为经济、可行。  相似文献   

16.
采用HL-5000型横流CO2激光加工机在TC4钛合金表面激光熔覆TiC+Ti和TiC+Ti+F102复合涂层。通过SEM、EDAX、XRD、HXD-1000TMC型显微硬度计,HT-600型高温摩擦磨损试验机,分析了熔覆层的显微组织、成分、物相,测试了激光熔覆层的显微硬度和滑动摩擦磨损性能。结果表明,激光熔覆制备的TiC复合涂层与基体呈冶金结合,在TiC+Ti激光熔覆层中,熔覆层的组织是在Ti基体上分布着TiC树枝晶;在TiC+Ti+F102激光熔覆层中,TiC颗粒发生了部分溶解,熔覆层的组织是在Ti基和γ-Ni基的基体上分布着细小的TiC颗粒和TiC树枝晶。TiC+Ti激光熔覆层的硬度约为700 HV0.1,TiC+Ti+F102激光熔覆层的硬度约为800 HV0.1,两种复合涂层耐磨性均比TC4钛合金显著提高。  相似文献   

17.
从切削力、刀具磨损、表面粗糙度3方面进行实验研究,找出P20钢与718钢的切削共性,从而得到预硬型塑料模具钢的加工特性.结果表明,对主切削力影响较大的是切削深度和进给量;当切削速度超过80~90 m/min时,表面粗糙度明显降低;与45钢相比,这类模具钢的刀具耐用度较差,且刀具主要磨损形态是磨料磨损.  相似文献   

18.
1 Introduction Tindioxidefilmshavebeenwidelyusedasconductiveelectrodes,transparentcoatings,andheterojunctionsolarcells.SnO2filmswithdifferentstructurescanbeconstructedbychemicalvapordepositiononsubstratesofdifferenttemperatures.AboafandMarcotte[1]pr…  相似文献   

19.
Fluidized chemical vapor deposition (FCVD) technology was developed for coating SnO2 thin film on ultrafine Al2O3 particles.Transmission electron microscopy (TEM) and high-resolution electron microscopy (HREM) analyses demonstrated that SnO2 films with different structures were deposited through controlling the coating temperature, reactant concentration, etc.. Nanocrystalline SnO2 film was formed at 572.15K by gas phase reaction of SnCl4 and H2O.Electron probe microanalyser (EPMA) and energy dispersive spectrometer (EDS) analyses indicated that the distribution of nanocrystalline SnO2 over inner and outer part of the Al2O3 agglomerates was homogeneous.  相似文献   

20.
以占空比、脉冲频率、电流密度、镀液温度为优化工艺参数,以镀层表面硬度、结合强度、磨损量、腐蚀速率为综合优化工艺目标,运用改进的TOPSIS法对脉冲电沉积Ni-P-W合金工艺参数进行优化。优化结果为:占空比30%、脉冲频率250 Hz、电流密8 A/dm2、镀液温度60℃。采用优化工艺参数进行脉冲电沉积Ni-P-W合金与最优试验设计组相比,表面硬度提高了8.14%,结合强度提高了5.32%,磨损量减小了4.26%,腐蚀速率减小了6.25%。  相似文献   

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